Benzyl diethylborinate

Base Information

• Chemical Name: Benzyl diethylborinate
• CAS No.: 93130-39-3
• Molecular Formula: C11H17BO
• Molecular Weight: 176.066
• DSSTox Substance ID: DTXSID40549968
• Mol file: 93130-39-3.mol

Synonyms:Benzyl diethylborinate;93130-39-3;DTXSID40549968

Chemical Property of Benzyl diethylborinate

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 176.1372453
• Heavy Atom Count: 13
• Complexity: 117

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B(CC)(CC)OCC1=CC=CC=C1

Technology Process of Benzyl diethylborinate

There total 2 articles about Benzyl diethylborinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethyl borane (97-94-9) + benzaldehyde (100-52-7) → ethene (74-85-1) + diethyl-benzyloxy-borane (93130-39-3)

Guidance literature:

at 200 ℃;

Reference yield:

Diethylborane (5518-25-2) + benzyl alcohol (100-51-6,185532-71-2) → diethyl-benzyloxy-borane (93130-39-3)

Guidance literature:

Reference yield:

diethyl phosphorylchloridite (589-57-1) + diethyl-benzyloxy-borane (93130-39-3) → benzyl diethyl phosphite (2768-31-2)

Guidance literature:

With triethylamine; acetylacetone; Multistep reaction; 1.) THF, -30 deg C, 2 h; 2.) 0 deg C, 2 h; RT, 5 h;

upstream raw materials:

triethyl borane

benzaldehyde

Diethylborane

benzyl alcohol

Downstream raw materials:

benzyl diethyl phosphite

benzyloxydiphenylphosphine

benzyl diethyl phosphate

(benzyloxy)di(phenyl)phosphine oxide