Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl-

Base Information

• Chemical Name: Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl-
• CAS No.: 93215-51-1
• Molecular Formula: C9H20O2Si
• Molecular Weight: 188.342
• DSSTox Substance ID: DTXSID40456562
• Nikkaji Number: J633.560H
• Wikidata: Q82279113
• Mol file: 93215-51-1.mol

Synonyms:Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl-;SCHEMBL8708806;DTXSID40456562;1-tert-Butoxyethenyloxytrimethylsilane

Chemical Property of Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 188.123256411
• Heavy Atom Count: 12
• Complexity: 162

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C)(C)OC(=C)O[Si](C)(C)C

Technology Process of Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl-

There total 1 articles about Silane, [[1-(1,1-dimethylethoxy)ethenyl]oxy]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + acetic acid tert-butyl ester (540-88-5) → tert-butyl (trimethylsilyl)acetate (41108-81-0) + 1-tert-butoxy-1-(trimethylsiloxy)ethylene (93215-51-1)

Guidance literature:

acetic acid tert-butyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;

chloro-trimethyl-silane; at -35 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ja107314p

Reference yield: 99.0%

N-benzylidene benzylamine (780-25-6) + 1-tert-butoxy-1-(trimethylsiloxy)ethylene (93215-51-1) → tert-Butyl 3-(N-benzylamino)-3-phenylpropanoate (167628-35-5)

Guidance literature:

With tris(pentafluorophenyl)borate; In toluene; 1.) -78 deg C, 13 h, 2.) 25 deg C, 8.5 h;

DOI:10.1246/bcsj.68.1721

Reference yield: 99.0%

1-tert-butoxy-1-(trimethylsiloxy)ethylene (93215-51-1) + N-(2-methylbutylidene)benzylamine (93965-52-7) → t-butyl 3-(benzylamino)-4-methylhexanoate

Guidance literature:

With tris(pentafluorophenyl)borate; In toluene; 1.) -78 deg C, 24 h, 2.) 25 deg C, 2 h;

DOI:10.1246/bcsj.68.1721

upstream raw materials:

chloro-trimethyl-silane

acetic acid tert-butyl ester

Downstream raw materials:

2-chloropyridine

2-fluoropyridine

tert-butyl 2-(pyridin-2-yl)acetate

tert-butyl (3R,αS)-3-[N-(α-methylbenzyl)amino]-3-phenylpropanoate