6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole

Base Information

• Chemical Name: 6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole
• CAS No.: 94358-39-1
• Molecular Formula: C12H14O4
• DSSTox Substance ID: DTXSID00538191
• Wikidata: Q82413439
• Mol file: 94358-39-1.mol

Synonyms:94358-39-1;6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole;SCHEMBL24242248;DTXSID00538191

Chemical Property of 6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 222.08920892
• Heavy Atom Count: 16
• Complexity: 253

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C2=C(C=C1C3CC3)OCO2)OC

Technology Process of 6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole

There total 2 articles about 6-Cyclopropyl-4,5-dimethoxy-2H-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dillapiole (484-31-1) → 4.5-Dimethoxy-6-(1-propenyl)-1,3-benzodioxol (17672-89-8) + 2,3-dimethoxy-4,5-methylenedioxybenzaldehyde (23731-65-9) + dihydrodillapiole (38174-54-8) + 1-Cyclopropyl-2,3-dimethoxy-4,5-methylenedioxybenzene (94358-39-1)

Guidance literature:

In methanol; for 72h; Further byproducts given; Irradiation;

Reference yield:

methanol (67-56-1) + dillapiole (484-31-1) → 4.5-Dimethoxy-6-(1-propenyl)-1,3-benzodioxol (17672-89-8) + 2,3-dimethoxy-4,5-methylenedioxybenzaldehyde (23731-65-9) + dihydrodillapiole (38174-54-8) + Dillapional (38971-74-3) + 1-Cyclopropyl-2,3-dimethoxy-4,5-methylenedioxybenzene (94358-39-1) + 4,5-Dimethoxy-6-(1-methoxy-propyl)-benzo[1,3]dioxole (69232-77-5)

Guidance literature:

With oxygen; for 72h; Product distribution; Irradiation; other substrate: isodillapiole, other solvent (in presence of rose bengal on silica gel): CCl₄;

upstream raw materials:

methanol

dillapiole