6,7-dimethoxy-1,3-benzodioxole-5-carbaldehyde

Base Information

• Chemical Name: 6,7-dimethoxy-1,3-benzodioxole-5-carbaldehyde
• CAS No.: 23731-65-9
• Molecular Formula: C10H10 O5
• Molecular Weight: 210.1834
• Mol file: 23731-65-9.mol

Synonyms:Benzaldehyde,2,3-dimethoxy-4,5-(methylenedioxy)- (8CI); Dillapiole aldehyde

Chemical Property of 6,7-dimethoxy-1,3-benzodioxole-5-carbaldehyde

Chemical Property:

• Vapor Pressure: 0.000272mmHg at 25°C
• Boiling Point: 322.8°Cat760mmHg
• Flash Point: 143.3°C
• Density: 1.311g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6,7-dimethoxy-1,3-benzodioxole-5-carbaldehyde

There total 19 articles about 6,7-dimethoxy-1,3-benzodioxole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4.5-Dimethoxy-6-(1-propenyl)-1,3-benzodioxol (17672-89-8) → 2,3-dimethoxy-4,5-methylenedioxybenzaldehyde (23731-65-9) + dillapionic acid (22027-56-1) + dihydroxyisodillapiole (87687-11-4)

Guidance literature:

With potassium permanganate; magnesium sulfate; In acetone; at 0 ℃;

Reference yield: 80.0%

4,5-dimethoxy-6-(prop-1-en-1-yl)benzo[1,3]dioxole (23731-63-7) → 2,3-dimethoxy-4,5-methylenedioxybenzaldehyde (23731-65-9)

Guidance literature:

4,5-dimethoxy-6-(prop-1-en-1-yl)benzo[1,3]dioxole; With ozone; In pyridine; methanol; chloroform; at -25 ℃;

With water;

DOI:10.1007/s11172-007-0389-1

Reference yield: 78.0%

4.5-Dimethoxy-6-(1-propenyl)-1,3-benzodioxol (17672-89-8) → 2,3-dimethoxy-4,5-methylenedioxybenzaldehyde (23731-65-9)

Guidance literature:

With potassium permanganate; carbon dioxide; In water; acetone; at 0 ℃; for 0.333333h;

upstream raw materials:

3,4-dimethoxy-1,2-methylenedioxybenzene

N,N-dimethyl-formamide

methanol

dillapiole

Downstream raw materials:

6-allyloxy-4,5-dimethoxy-1,3-benzodioxole

2,3-dimethoxysesamyl n-propylether

2,3-dimethoxysesamyl β-methallylether

2,3-dimethoxysesamyl β-cyanoethylether

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