2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol

Base Information

• Chemical Name: 2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol
• CAS No.: 95684-29-0
• Molecular Formula: C5H10Cl2O4
• Molecular Weight: 205.038
• DSSTox Substance ID: DTXSID00538818
• Mol file: 95684-29-0.mol

Synonyms:95684-29-0;SCHEMBL20510006;2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol;DTXSID00538818

Chemical Property of 2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol

Chemical Property:

• XLogP3: 0.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 203.9956142
• Heavy Atom Count: 11
• Complexity: 92.6

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC(CCl)OOC(CCl)O

Technology Process of 2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol

There total 1 articles about 2-Chloro-1-[(2-chloro-1-methoxyethyl)peroxy]ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methanol (67-56-1) + trans-1,4-dichlorobut-2-ene (110-57-6) → 2-chloro-1-methoxyethyl hydroperoxide (87894-31-3) + 2-Chlor-1-methoxyethanol (65652-26-8) + 2-chloro-1-hydroxyethyl 2-chloro-1-methoxyethyl peroxide (95684-29-0)

Guidance literature:

With ozone; - 15 deg C to -50 deg C;

Reference yield:

2-chloro-1-hydroxyethyl 2-chloro-1-methoxyethyl peroxide (95684-29-0) → chloroacetaldehyde dimethyl acetal (97-97-2) + methyl chloroacetate (96-34-4)

Guidance literature:

With hydrogenchloride; In methanol; chloroform-d1; Yield given. Yields of byproduct given; 1.) 40 deg C, 16 h, 2.) 60 deg C, 12 h;

Reference yield:

methanol (67-56-1) + 2-chloro-1-hydroxyethyl 2-chloro-1-methoxyethyl peroxide (95684-29-0) → chloroacetaldehyde dimethyl acetal (97-97-2) + methyl chloroacetate (96-34-4)

Guidance literature:

With hydrogenchloride; In chloroform-d1; Yield given. Yields of byproduct given; 1.) 40 deg C, 16 h, 2.) 60 deg C, 12 h;

upstream raw materials:

methanol

trans-1,4-dichlorobut-2-ene

Downstream raw materials:

chloroacetaldehyde dimethyl acetal

methyl chloroacetate