4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide

Base Information

Chemical Name:4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide
CAS No.:6949-53-7
Molecular Formula:C14H13 N3 O4 S
Molecular Weight:319.3357
Hs Code.:
DSSTox Substance ID:DTXSID00417876

Synonyms:DTXSID00417876;6949-53-7;4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide

Suppliers and Price of 4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide

Chemical Property:

Boiling Point:499.6°Cat760mmHg
Flash Point:256°C
Density:1.35g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:319.06267708
Heavy Atom Count:22
Complexity:507

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=NNS(=O)(=O)C1=CC=C(C=C1)[N+](=O)[O-])C2=CC=CC=C2
Isomeric SMILES:C/C(=N\NS(=O)(=O)C1=CC=C(C=C1)[N+](=O)[O-])/C2=CC=CC=C2

Technology Process of 4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide

There total 2 articles about 4-Nitro-N'-[(1E)-1-phenylethylidene]benzene-1-sulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2937-05-5
4-nitrobenzenesulfonohydrazide

: 98-86-2
acetophenone

: 6949-53-7
(E)-4-nitro-N'-(1-phenylethylidene)benzenesulfonohydrazide

Guidance literature:: With hydrogenchloride; Ambient temperature;
DOI:10.1246/bcsj.58.377

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 6949-53-7
(E)-4-nitro-N'-(1-phenylethylidene)benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 100percent hydrazine hydrate

2: 71 percent / 1 M HCl / Ambient temperature

With hydrogenchloride; hydrazine hydrate;
DOI:10.1246/bcsj.58.377

Reference yield: 70.0%

: 1459246-62-8
4-phenyl-4-vinyl-1,3-dioxolan -2-one

: 6949-53-7
(E)-4-nitro-N'-(1-phenylethylidene)benzenesulfonohydrazide

: N-((Z)-4-hydroxy-3-phenylbut-2-en-1-yl)-4-nitro-N'-((E)-1-phenylethylidene)benzenesulfonohydrazide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In acetonitrile; at 80 ℃; for 2h; stereoselective reaction; Sealed tube;
DOI:10.1002/chem.201805295