N-(4,5-dibromo-2-methoxyphenyl)acetamide

Base Information

Chemical Name:N-(4,5-dibromo-2-methoxyphenyl)acetamide
CAS No.:95970-11-9
Molecular Formula:C9H9Br2NO2
Molecular Weight:322.984
Hs Code.:
DSSTox Substance ID:DTXSID701276801
Nikkaji Number:J314.065B
Mol file:95970-11-9.mol

Synonyms:N-(4,5-dibromo-2-methoxyphenyl)acetamide;DTXSID701276801;95970-11-9;N-(2-Methoxy-4,5-dibromophenyl)acetamide;SR-01000210021;SR-01000210021-1

Suppliers and Price of N-(4,5-dibromo-2-methoxyphenyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(4,5-dibromo-2-methoxyphenyl)acetamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:322.89795
Heavy Atom Count:14
Complexity:213

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=CC(=C(C=C1OC)Br)Br

Technology Process of N-(4,5-dibromo-2-methoxyphenyl)acetamide

There total 2 articles about N-(4,5-dibromo-2-methoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 93-26-5
2-methoxyacetanilide

: 95970-11-9
2-Acetamido-4,5-dibromoanisole

Guidance literature:: With bromine; In acetic acid;

Reference yield:

: 143360-01-4
N-(4-bromo-2-methoxyphenyl)acetamide

: 7726-95-6
bromine

: 64-19-7,77671-22-8
acetic acid

: 95970-11-9
2-Acetamido-4,5-dibromoanisole

Guidance literature:: DOI:10.1021/jo01133a009

Reference yield:

: 95970-11-9
2-Acetamido-4,5-dibromoanisole

: 95970-10-8
2,4,5-tribromo-anisole

Guidance literature:: Multi-step reaction with 2 steps

1: 73.6 percent / conc. HCl / ethanol / 3 h / Heating

2: 1.) aq. H₂SO₄, NaNO₂, 2.) Cu₂Br₂, conc. HBr; / 1.) acetic acid, 0 deg C, 30 min, 2.) 0 deg C, 30 min, 3.) from 0 deg C, to 100 deg C, 1.5 h;

With copper(I) bromide; hydrogenchloride; sulfuric acid; hydrogen bromide; sodium nitrite; In ethanol;