di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

Base Information

Chemical Name:di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate
CAS No.:913239-30-2
Molecular Formula:C₃₇H₄₁N₄O₉P
Molecular Weight:716.728
Hs Code.:

Synonyms:di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

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Technology Process of di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

There total 5 articles about di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 621-84-1
O-benzyl carbamate

: 222610-50-6
tris-(4-acetamidophenyl)phosphite

: 695171-91-6
4-(tert-butyloxycarbonylamino)phenylacetaldehyde

: 913239-30-2
di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

Guidance literature:: With yttrium(III) trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 4h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/d1ra07718j

Reference yield: 20.0%

: 913239-30-2
di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

Guidance literature:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 913239-30-2
di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / dioxane / 20 °C

2: Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

3: Cu(OTf)2 / CH₂Cl₂ / 4 h / 20 °C

With copper(II) bis(trifluoromethanesulfonate); Dess-Martin periodane; triethylamine; In 1,4-dioxane; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1021/jm060622g