Methyl3-hydroxy-5-iodobenzoate

Base Information

Chemical Name:Methyl3-hydroxy-5-iodobenzoate
CAS No.:50765-22-5
Molecular Formula:C8H7IO3
Molecular Weight:278.046
Hs Code.:2918290000
Mol file:50765-22-5.mol

Synonyms:Benzoic acid, 3-hydroxy-5-iodo-, methyl ester; Methyl 3-hydroxy-5-iodobenzoate

Suppliers and Price of Methyl3-hydroxy-5-iodobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Methyl3-hydroxy-5-iodobenzoate
25mg
$ 105.00

Crysdot
Methyl3-hydroxy-5-iodobenzoate 97%
1g
$ 480.00

American Custom Chemicals Corporation
METHYL-3-HYDROXY-5-IODOBENZOATE 95.00%
5MG
$ 496.20

Alichem
Methyl3-hydroxy-5-iodobenzoate
1g
$ 922.18

AK Scientific
Methyl3-hydroxy-5-iodobenzoate
1g
$ 1345.00

Total 17 raw suppliers

Chemical Property of Methyl3-hydroxy-5-iodobenzoate

Chemical Property:

Vapor Pressure:5.95E-06mmHg at 25°C
Refractive Index:1.633
Boiling Point:368.6°C at 760 mmHg
Flash Point:176.7°C
PSA：46.53000
Density:1.88g/cm³
LogP:1.78340
Storage Temp.:2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

Methyl3-hydroxy-5-iodobenzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Methyl 3-hydroxy-5-iodobenzoate

Technology Process of Methyl3-hydroxy-5-iodobenzoate

There total 4 articles about Methyl3-hydroxy-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 67-56-1
methanol

: 50765-21-4
3-hydroxy-5-iodobenzoic acid

: 50765-22-5
methyl 3-hydroxy-5-iodobenzoate

Guidance literature:: With thionyl chloride; at 0 - 23 ℃; for 16.5h;
DOI:10.1021/acs.jmedchem.6b00044

Reference yield:

: 6313-17-3
3-iodo-5-nitro-benzoic acid

: 50765-22-5
methyl 3-hydroxy-5-iodobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: (i) SOCl₂, (ii) /BRN= 1098229/

2: SnCl₂, aq. HCl

3: (i) aq. NaNO₂, H₂SO₄, (ii) aq. H₂SO₄

With hydrogenchloride; tin(ll) chloride;
DOI:10.1021/jm00264a023

Reference yield:

: 50765-19-0
methyl 3-iodo-5-nitrobenzoate

: 50765-22-5
methyl 3-hydroxy-5-iodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂, aq. HCl

2: (i) aq. NaNO₂, H₂SO₄, (ii) aq. H₂SO₄

With hydrogenchloride; tin(ll) chloride;
DOI:10.1021/jm00264a023