5-Bromo-3-cyano-2-methoxypyridine

Base Information

Chemical Name:5-Bromo-3-cyano-2-methoxypyridine
CAS No.:941294-54-8
Molecular Formula:C7H5BrN2O
Molecular Weight:213.033
Hs Code.:2933399090
Mol file:941294-54-8.mol

Synonyms:5-bromo-2-methoxypyridine-3-carbonitrile

Suppliers and Price of 5-Bromo-3-cyano-2-methoxypyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Bromo-2-methoxynicotinonitrile
250mg
$ 55.00

TRC
5-Bromo-2-methoxynicotinonitrile
100mg
$ 45.00

TRC
5-Bromo-2-methoxynicotinonitrile
500mg
$ 65.00

SynQuest Laboratories
5-Bromo-2-methoxynicotinonitrile 98%
5 g
$ 245.00

SynQuest Laboratories
5-Bromo-2-methoxynicotinonitrile 98%
1 g
$ 59.00

Sigma-Aldrich
5-Bromo-2-methoxypyridine-3-carbonitrile 97%
1g
$ 69.10

Frontier Specialty Chemicals
5-Bromo-3-cyano-2-methoxypyridine 96%
5g
$ 250.00

Frontier Specialty Chemicals
5-Bromo-3-cyano-2-methoxypyridine 96%
1g
$ 63.00

Crysdot
5-Bromo-2-methoxynicotinonitrile 95+%
5g
$ 168.00

Chemenu
5-Bromo-2-methoxynicotinonitrile 95%
25g
$ 757.00

Total 31 raw suppliers

Chemical Property of 5-Bromo-3-cyano-2-methoxypyridine

Chemical Property:

Vapor Pressure:0.00863mmHg at 25°C
Melting Point:110-115°C
Boiling Point:267℃
PKA:-2.40±0.20(Predicted)
Flash Point:115℃
PSA：45.91000
Density:1.65
LogP:1.72438
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-2-methoxynicotinonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi,T
Hazard Codes:Xi,T
Statements: 25-36/37/38
Safety Statements: 26-36-45

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Bromo-3-cyano-2-methoxypyridine

There total 2 articles about 5-Bromo-3-cyano-2-methoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 7254-34-4
2-methoxy-3-cyanopyridine

: 941294-54-8
5-bromo-2-methoxypyridine-3-carbonitrile

Guidance literature:: With bromine; sodium acetate; In acetic acid; at 0 - 70 ℃;

Reference yield:

: 6602-54-6
2-chloro-3-pyridinecarbonitrile

: 941294-54-8
5-bromo-2-methoxypyridine-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / 0.17 h / 20 °C

1.2: 0 - 25 °C

1.3: 0 °C

2.1: sodium acetate; bromine / acetic acid / 0 - 70 °C

With bromine; sodium acetate; sodium; In acetic acid;

Reference yield: 91.0%

: 941294-54-8
5-bromo-2-methoxypyridine-3-carbonitrile

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 2-methoxy-5-[4-(trifluoromethyl)phenyl]pyridine-3-carbonitrile

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In 1,4-dioxane; water; at 100 ℃; for 0.333333h; Microwave irradiation;