methyl 2-(4-formyl-3-hydroxyphenyl)acetate

Base Information

• Chemical Name: methyl 2-(4-formyl-3-hydroxyphenyl)acetate
• CAS No.: 1257397-40-2
• Molecular Formula: C10H10O4
• Molecular Weight: 194.187
• Hs Code.: 2918990090
• Mol file: 1257397-40-2.mol

Synonyms:Methyl 2-(4-forMyl-3-hydroxyphenyl)acetate;Benzeneacetic acid, 4-formyl-3-hydroxy-, methyl ester

Chemical Property of methyl 2-(4-formyl-3-hydroxyphenyl)acetate

Chemical Property:

• PSA: 63.60000
• LogP: 0.92020
• Storage Temp.: 2-8°C

Purity/Quality:

95% Min ^*data from raw suppliers

Methyl2-(4-formyl-3-hydroxyphenyl)acetate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 2-(4-formyl-3-hydroxyphenyl)acetate

There total 1 articles about methyl 2-(4-formyl-3-hydroxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 3-hydroxy-benzeneacetic acid, methyl ester (42058-59-3) → methyl 2-(4-formyl-3-hydroxyphenyl)acetate (1257397-40-2)

Guidance literature:

3-hydroxy-benzeneacetic acid, methyl ester; With triethylamine; In acetonitrile; for 0.166667h;

With magnesium chloride; In acetonitrile; for 1.75h;

formaldehyd;

Reference yield: 82.0%

4-Trifluormethyl-piperidin (657-36-3) + methyl 2-(4-formyl-3-hydroxyphenyl)acetate (1257397-40-2) + 4-fluoroboronic acid (1765-93-1) → methyl 2-(4-((4-fluorophenyl)(4-(trifluoromethyl)piperidin-1-yl)methyl)-3-hydroxyphenyl)acetate (1257397-68-4)

Guidance literature:

In 4-methyl-1,2,3-trifluorobenzene; at 120 ℃; for 0.166667h; microwave irradiation;

Reference yield: 78.0%

trifluoromethylsulfonic anhydride (358-23-6) + methyl 2-(4-formyl-3-hydroxyphenyl)acetate (1257397-40-2) → methyl 2-(4-formyl-3-(trifluoromethylsulfonyloxy)phenyl)acetate (1257397-41-3)

Guidance literature:

With pyridine; dmap; In dichloromethane; at -12 - 0 ℃; Product distribution / selectivity; Cooling with methanol-ice;

upstream raw materials:

formaldehyd

3-hydroxy-benzeneacetic acid, methyl ester

Downstream raw materials:

methyl 2-(4-formyl-3-(trifluoromethylsulfonyloxy)phenyl)acetate

methyl 2-(4-((4-fluorophenyl)(4-(trifluoromethyl)piperidin-1-yl)methyl)-3-hydroxyphenyl)acetate

2-(4'-tert-butyl-6-((4-fluorophenyl)(4-(trifluoromethyl)piperidin-1-yl)methyl)biphenyl-3-yl)acetic acid

methyl 2-(4-((4-fluorophenyl)(4-(trifluoromethyl)piperidin-1-yl)methyl)-3-(trifluoromethylsulfonyloxy)phenyl)acetate

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