NSC 304613

Base Information

• Chemical Name: NSC 304613
• CAS No.: 210035-02-2
• Molecular Formula: C14H10N2O
• Molecular Weight: 222.24200
• Mol file: 210035-02-2.mol

Synonyms:

Chemical Property of NSC 304613

Chemical Property:

• Melting Point: 135℃
• PSA: 34.37000
• LogP: 2.56530
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Imidazo[1,2-a]pyridin-3-yl(phenyl)methanone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NSC 304613

There total 28 articles about NSC 304613 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N,N-dimethyl-N'-pyridin-2-yl-formamidine (17175-39-2) + α-bromoacetophenone (70-11-1) → (1H-imidazo[1,2-a]pyridin-3-yl)(phenyl)methanone (210035-02-2)

Guidance literature:

at 65 - 70 ℃; Inert atmosphere;

DOI:10.1515/HC.2010.16.2-3.99

Reference yield: 89.0%

1-phenyl-3-(pyridin-2-ylamino)prop-2-en-1-one → (1H-imidazo[1,2-a]pyridin-3-yl)(phenyl)methanone (210035-02-2)

Guidance literature:

With copper(l) iodide; In dimethyl sulfoxide; at 100 ℃; for 12h;

Reference yield: 89.0%

(Z)-1-phenyl-3-(pyridin-2-ylamino)prop-2-en-1-one (15753-55-6) → (1H-imidazo[1,2-a]pyridin-3-yl)(phenyl)methanone (210035-02-2)

Guidance literature:

With copper(l) iodide; In dimethyl sulfoxide; at 100 ℃; for 12h; Solvent; Temperature; Reagent/catalyst;

DOI:10.1016/j.tetlet.2016.05.064

upstream raw materials:

ethanol

imidazo[1,2-a]pyridine

benzoyl chloride

3-benzoyl-2-methylthioimidazo<1,2-a>pyridine

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