6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine

Base Information

• Chemical Name: 6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine
• CAS No.: 24603-30-3
• Molecular Weight: 150.18
• DSSTox Substance ID: DTXSID50511792
• Mol file: 24603-30-3.mol

Synonyms:6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine;24603-30-3;6-methoxy-5-azaindoline;SCHEMBL3034518;DTXSID50511792;1H-Pyrrolo[3,2-c]pyridine, 2,3-dihydro-6-Methoxy-;6-methoxy-2, 3-dihydro-1h-pyrrolo[3, 2-c]pyridine

Chemical Property of 6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 150.079312947
• Heavy Atom Count: 11
• Complexity: 140

Purity/Quality:

99% ^*data from raw suppliers

6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=NC=C2CCNC2=C1

Technology Process of 6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine

There total 2 articles about 6-Methoxy-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.3%

sodium methylate (124-41-4) + 6-chloro-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine (23596-25-0) → 6-methoxy-5-azaindoline (24603-30-3)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; for 6h;

DOI:10.1007/BF00506995

Reference yield:

→ 6-methoxy-5-azaindoline (24603-30-3)

Guidance literature:

6-Chlor-5-aza-indolin, K-methylat (190grad, 15 Std.);

DOI:10.1007/BF00471161

Reference yield: 40.7%

6-methoxy-5-azaindoline (24603-30-3) → 6-methoxy-5-azaindole (80862-08-4)

Guidance literature:

With activated γ-manganese dioxide; In benzene;

DOI:10.1007/BF00506995

upstream raw materials:

sodium methylate

6-chloro-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine

Downstream raw materials:

6-methoxy-5-azaindole

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