2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl-

Base Information

Chemical Name:2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl-
CAS No.:90537-20-5
Molecular Formula:C9H8ClNO
Molecular Weight:181.62
Hs Code.:
Mol file:90537-20-5.mol

Synonyms:5-chloro-3-methylindolin-2-one;5-chloro-3-methyl-1,3-dihydro-indol-2-one;5-chloro-3-methyl-1-phenyl-1H-pyrazole;5-chloro-3-methyl-2-indolinone;5-Chlor-3-methyl-oxindol;5-Chlor-3-methyl-1-phenyl-1H-pyrazol;3-Methyl-5-chlorooxindole;

Suppliers and Price of 2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
2H-INDOL-2-ONE,5-CHLORO-1,3-DIHYDRO-3-METHYL- 95
2g
$ 1417.00

American Custom Chemicals Corporation
2H-INDOL-2-ONE, 5-CHLORO-1,3-DIHYDRO-3-METHYL- 95.00%
5MG
$ 495.54

Total 7 raw suppliers

Chemical Property of 2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl-

Chemical Property:

PSA：32.59000
LogP:2.48070

Purity/Quality:

97% ^*data from raw suppliers

2H-INDOL-2-ONE,5-CHLORO-1,3-DIHYDRO-3-METHYL- 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl-

There total 10 articles about 2H-Indol-2-one, 5-chloro-1,3-dihydro-3-Methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 17630-75-0
5-chloro-indolin-2-one

: 90537-20-5
5-chloro-3-methyl-2-indolinone

Guidance literature:: 5-chloro-indolin-2-one; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

methyl halide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201700851

Reference yield: 86.0%

: 201230-82-2
carbon monoxide

: 112768-02-2
4-chloro-1-nitro-2-vinylbenzene

: 90537-20-5
5-chloro-3-methyl-2-indolinone

Guidance literature:: With boric acid; triphenylphosphine; palladium dichloride; In tetrahydrofuran; at 80 ℃; for 20h; under 26601.8 Torr; regioselective reaction;
DOI:10.1021/acscatal.8b02863

Reference yield: 85.0%

: 67-56-1
methanol

: 17630-75-0
5-chloro-indolin-2-one

: 90537-20-5
5-chloro-3-methyl-2-indolinone

Guidance literature:: With trimethylamine-N-oxide; tricarbonyl(η⁴-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron; potassium carbonate; at 110 ℃; for 24h;
DOI:10.1021/acscatal.8b02158