2,6-Dibromobenzyl acetate

Base Information

• Chemical Name: 2,6-Dibromobenzyl acetate
• CAS No.: 1147858-83-0
• Molecular Formula: C9H8Br2O2
• Molecular Weight: 307.969
• Hs Code.: 2915390090
• Mol file: 1147858-83-0.mol

Synonyms:2,6-dibroMobenzyl acetate;Acetic acid 2,6-dibromobenzyl ester

Chemical Property of 2,6-Dibromobenzyl acetate

Chemical Property:

• Boiling Point: 311.4±27.0 °C(Predicted)
• PSA: 26.30000
• Density: 1.763±0.06 g/cm3(Predicted)
• LogP: 3.27470
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,6-Dibromobenzylacetate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Dibromobenzyl acetate

There total 3 articles about 2,6-Dibromobenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,6-dibromobenzyl bromide (93701-32-7) + sodium acetate (127-09-3) → acetic acid 2,6-dibromobenzyl ester (1147858-83-0)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; for 1.75h;

Reference yield: 88.0%

2,6-dibromobenzyl bromide (93701-32-7) + potassium acetate (127-08-2) → acetic acid 2,6-dibromobenzyl ester (1147858-83-0)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;

Reference yield:

2,6-dibromotoluene (69321-60-4) → acetic acid 2,6-dibromobenzyl ester (1147858-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 14 h / 80 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; N,N-dimethyl-formamide;

upstream raw materials:

2,6-dibromobenzyl bromide

sodium acetate

potassium acetate

2,6-dibromotoluene

Downstream raw materials:

2,6-diethylbenzyl acetate

2,6-diethylbenzyl alcohol

acetic acid 2-bromo-6-(6-tert-butyl-1-oxo-3,4-dihydro-1H-isoquinolin-2-yl)-benzyl ester

acetic acid 2-bromo-6-(6-dimethylamino-1-oxo-3,4-dihydro-1H-isoquinolin-2-yl)benzyl ester