Ethyl 2-broMo-5-iodobenzoate

Base Information

• Chemical Name: Ethyl 2-broMo-5-iodobenzoate
• CAS No.: 1208075-44-8
• Molecular Formula: C9H8BrIO2
• Molecular Weight: 354.97
• Hs Code.: 2916399090
• Mol file: 1208075-44-8.mol

Synonyms:Ethyl 2-broMo-5-iodobenzoate;2-Bromo-5-iodobenzoic acid ethyl ester;Benzoic acid, 2-bromo-5-iodo-, ethyl ester

Chemical Property of Ethyl 2-broMo-5-iodobenzoate

Chemical Property:

• Boiling Point: 341.79 °C at 760 mmHg
• Flash Point: 160.509 °C
• PSA: 26.30000
• Density: 1.949 g/cm³
• LogP: 3.23040
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-5-iodo-benzoicacidethylester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 2-broMo-5-iodobenzoate

There total 1 articles about Ethyl 2-broMo-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-bromo-5-iodobenzoic acid (25252-00-0) + ethyl iodide (75-03-6) → ethyl 2-bromo-5-iodobenzoate (1208075-44-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1021/acs.oprd.9b00180

Reference yield: 85.0%

zinc(II) cyanide (557-21-1) + ethyl 2-bromo-5-iodobenzoate (1208075-44-8) → ethyl 2-bromo-5-cyanobenzoate

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 70 ℃; for 17h; Inert atmosphere;

DOI:10.1021/acs.oprd.9b00180

Reference yield: 77.0%

ethyl 2-bromo-5-iodobenzoate (1208075-44-8) + bromo(2-ethoxy-2-oxoethyl)zinc (5764-82-9) → ethyl 2-bromo-5-(2-ethoxy-2-oxoethyl)benzoate (1552290-13-7)

Guidance literature:

With 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 65 ℃; for 3h; chemoselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1016/j.tet.2013.12.053

upstream raw materials:

2-bromo-5-iodobenzoic acid

ethyl iodide

Downstream raw materials:

ethyl 2-bromo-5-(2-ethoxy-2-oxoethyl)benzoate

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