3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylidene]-5-phenyl-

Base Information

• Chemical Name: 3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylidene]-5-phenyl-
• CAS No.: 768377-92-0
• Molecular Formula: C₃₄H₂₇N₃O₂
• Molecular Weight: 509.607

Synonyms:1H-Pyrrol-2-amine, 3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylide ne]-5-phenyl-;

Chemical Property of 3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylidene]-5-phenyl-

Chemical Property:

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Technology Process of 3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylidene]-5-phenyl-

There total 3 articles about 3-(4-methoxyphenyl)-N-[3-(4-methoxyphenyl)-5-phenyl-2H-pyrrol-2-ylidene]-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → [3-(4-methoxyphenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-methoxyphenyl)-5-phenylpyrrol-2-ylidene]amine (768377-92-0)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water

2: diethylamine / methanol / 24 h / Reflux

3: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; diethylamine; potassium hydroxide; In methanol; ethanol; water; butan-1-ol;

DOI:10.1021/ic300709n

Reference yield:

acetophenone (98-86-2) → [3-(4-methoxyphenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-methoxyphenyl)-5-phenylpyrrol-2-ylidene]amine (768377-92-0)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water

2: diethylamine / methanol / 24 h / Reflux

3: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; diethylamine; potassium hydroxide; In methanol; ethanol; water; butan-1-ol;

DOI:10.1021/ic300709n

Reference yield:

3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (959-33-1) → [3-(4-methoxyphenyl)-5-phenyl-1H-pyrrol-2-yl][3-(4-methoxyphenyl)-5-phenylpyrrol-2-ylidene]amine (768377-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / methanol / 24 h / Reflux

2: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; triethylamine; In methanol; butan-1-ol; 1: |Michael Addition;

DOI:10.1039/d0pp00026d

upstream raw materials:

4-methoxy-benzaldehyde

acetophenone

3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one

Downstream raw materials:

C₃₄H₂₅Br₂N₃O₂

(triphenylphosphine)Cu(N(C₄HN(C₆H₅)C₆H₄OCH₃)2)

(triethylphosphine)Ag(N(C₄HN(C₆H₅)C₆H₄OCH₃)2)

(triphenylphosphine)Ag(N(C₄HN(C₆H₅)C₆H₄OCH₃)2)

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