4-CHLORO-5-FLUORO-2-NITROPHENOL

Base Information

• Chemical Name: 4-CHLORO-5-FLUORO-2-NITROPHENOL
• CAS No.: 345-25-5
• Molecular Formula: C6H3ClFNO3
• Molecular Weight: 191.546
• Hs Code.: 2908990000
• Mol file: 345-25-5.mol

Synonyms:4-CHLORO-5-FLUORO-2-NITROPHENOL;2-amino-4-chloro-5-fluorophenol;5-Chloro-4-fluoro-2-hydroxynitrobenzene;5-Chloro-4-fluoro-2-hydroxyaniline;2-Nitro-4-chloro-5-fluorophenol

Chemical Property of 4-CHLORO-5-FLUORO-2-NITROPHENOL

Chemical Property:

• PSA: 66.05000
• LogP: 2.61610
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4-Chloro-5-fluoro-2-nitrophenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-5-FLUORO-2-NITROPHENOL

There total 2 articles about 4-CHLORO-5-FLUORO-2-NITROPHENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-chloro-3-fluorophenol (348-60-7) → 4-chloro-5-fluoro-2-nitrophenol (345-25-5)

Guidance literature:

With tetrabutylammomium bromide; nitric acid; In water; 1,2-dichloro-ethane; at 20 ℃; for 4h;

Reference yield:

5-fluoro-2-nitrophenol (446-36-6) → 4-chloro-5-fluoro-2-nitrophenol (345-25-5)

Guidance literature:

With sodium hypochlorite;

Reference yield: 96.0%

4-chloro-5-fluoro-2-nitrophenol (345-25-5) + methyl iodide (74-88-4) → 1-chloro-2-fluoro-4-methoxy-5-nitrobenzene (1089280-66-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 60h;

upstream raw materials:

5-fluoro-2-nitrophenol

4-chloro-3-fluorophenol

Downstream raw materials:

1-chloro-2-fluoro-4-methoxy-5-nitrobenzene

ethyl [(4-chloro-5-fluoro-2-nitrophenyl)oxy]acetate

6-chloro-7-fluoro-3-(methylthio)-2H-1,4-benzoxazine

2-hydroxy-5-chloro-aniline

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