2-Methylpropanal phenyl hydrazone

Base Information

• Chemical Name: 2-Methylpropanal phenyl hydrazone
• CAS No.: 5570-70-7
• Molecular Formula: C10H14N2
• Molecular Weight: 162.235
• Mol file: 5570-70-7.mol

Synonyms:2-Methylpropanal phenyl hydrazone

Chemical Property of 2-Methylpropanal phenyl hydrazone

Chemical Property:

• Boiling Point: 90-100 °C(Press: 0.03 Torr)
• PKA: 14.66±0.10(Predicted)
• PSA: 24.39000
• Density: 0.93±0.1 g/cm3(Predicted)
• LogP: 2.81330

Purity/Quality:

99% ^*data from raw suppliers

1-(2-Methylpropylidene)-2-phenylhydrazine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methylpropanal phenyl hydrazone

There total 5 articles about 2-Methylpropanal phenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

isobutyraldehyde (78-84-2) + phenylhydrazine (100-63-0) → isobutyraldehyde phenylhydrazone (5570-70-7)

Guidance literature:

In toluene;

Reference yield:

phenylhydrazine hydrochloride (59-88-1) + isobutyraldehyde (78-84-2) → isobutyraldehyde phenylhydrazone (5570-70-7)

Guidance literature:

With potassium acetate; In methanol; at 80 ℃; for 0.0333333h; Inert atmosphere; Sealed tube;

DOI:10.1002/chem.201304302

Reference yield:

phenylhydrazine hydrochloride (59-88-1) + isobutyraldehyde (78-84-2) → isobutyraldehyde phenylhydrazone (5570-70-7) + C10H13(2)HN2 (1605332-64-6) + C10H12(2)H2N2 (1605332-65-7)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; potassium acetate; diphenyl acetylene; In methanol; at 80 ℃; for 0.75h; Inert atmosphere; Sealed tube;

DOI:10.1002/chem.201304302

upstream raw materials:

isobutyraldehyde

phenylhydrazine

Isobutyronitrile

phenylhydrazine hydrochloride

Downstream raw materials:

3-Methylindole

3,3-dimethylindolenine

3-Isopropyl-1,5-diphenyl-formazan

2,3-dimethylindole