6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

Base Information

Chemical Name:6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one
CAS No.:1232030-55-5
Molecular Formula:C10H10BrN3OS
Molecular Weight:300.179
Hs Code.:
Mol file:1232030-55-5.mol

Synonyms:6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

Suppliers and Price of 6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one 95%+
1g
$ 2940.00

Chemenu
6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one 95%+
250mg
$ 1176.00

Chemenu
6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one 95%+
100mg
$ 758.00

Total 3 raw suppliers

Chemical Property of 6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

Chemical Property:

PSA：73.08000
LogP:2.29580

Purity/Quality:

NLT 98% ^*data from raw suppliers

6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

There total 3 articles about 6-Bromo-8-ethyl-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 75-03-6
ethyl iodide

: 352328-87-1
6-bromo-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 1232030-55-5
6-bromo-8-ethyl-2-(methylthio)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 18h;

Reference yield: 76.0%

: 74-96-4
ethyl bromide

: 352328-87-1
6-bromo-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 1232030-55-5
6-bromo-8-ethyl-2-(methylthio)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: 6-bromo-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 50 ℃; for 0.5h;

ethyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 - 50 ℃; for 1.5h;

Reference yield:

: 211244-81-4
2-methanesulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 1232030-55-5
6-bromo-8-ethyl-2-(methylthio)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 50 °C

2.2: 1.5 h / 50 °C

With N-Bromosuccinimide; sodium hydride; In N,N-dimethyl-formamide; mineral oil;