TRIMETHYL BORATE-10B, 97 ATOM % 10B

Base Information

• Chemical Name: TRIMETHYL BORATE-10B, 97 ATOM % 10B
• CAS No.: 4832-27-3
• Molecular Formula: C3H9BO3
• Molecular Weight: 103.103
• Hs Code.: 28459000
• Mol file: 4832-27-3.mol

Synonyms:TRIMETHYL BORATE-10B, 97 ATOM % 10B;trimethyl borate-10B;Methyl borate-10B

Chemical Property of TRIMETHYL BORATE-10B, 97 ATOM % 10B

Chemical Property:

• Melting Point: −34 °C(lit.)
• Refractive Index: n20/D 1.357(lit.)
• Boiling Point: 68-69 °C(lit.)
• Flash Point: -8 °C
• PSA: 27.69000
• Density: 0.915 g/mL at 25 °C(lit.)
• LogP: -0.08950

Purity/Quality:

99% ^*data from raw suppliers

TRIMETHYL BORATE-10B 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn,F
• Statements: 10-21-11
• Safety Statements: 16

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRIMETHYL BORATE-10B, 97 ATOM % 10B

There total 2 articles about TRIMETHYL BORATE-10B, 97 ATOM % 10B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) → tris(methoxy)borane (4832-27-3)

Guidance literature:

With [10B]boric acid; Heating;

DOI:10.1002/(SICI)1099-1344(200001)43:1<97::AID-JLCR296>3.0.CO;2-D

Reference yield:

methanol (67-56-1) + sodium methylate (124-41-4) + boron trifluoride (15875-25-9) → tris(methoxy)borane (4832-27-3)

Guidance literature:

With calcium chloride; at 55 ℃; Temperature; Concentration; Kinetics;

DOI:10.14233/ajchem.2015.16895

Reference yield: 73.0%

2,3-dimethyl-2,3-butane diol (76-09-5) + tris(methoxy)borane (4832-27-3) + 5-bromo-1,3-xylene (556-96-7) → C14H21(10)BO2

Guidance literature:

5-bromo-1,3-xylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

trimethyl [10B]borate; In tetrahydrofuran; at 20 ℃;

2,3-dimethyl-2,3-butane diol; Further stages;

DOI:10.1002/ejic.202100949

upstream raw materials:

methanol

sodium methylate

boron trifluoride

Downstream raw materials:

[10B]boric acid