2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride

Base Information

Chemical Name:2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride
CAS No.:1389264-13-4
Molecular Formula:C₁₁H₁₇NO₂
Molecular Weight:195.261
Hs Code.:2933990090
Mol file:1389264-13-4.mol

Synonyms:2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride

Suppliers and Price of 2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylicacidmethylesterhydrochloride 95+%
100g
$ 440.00

Chemenu
2-aza-tricyclo[3.3.1.13,7]decane-5-carboxylicacidmethylesterhydrochloride 97%
100mg
$ 880.00

Total 11 raw suppliers

Chemical Property of 2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride

Chemical Property:

Boiling Point:268.2±33.0 °C(Predicted)
PKA:10.62±0.40(Predicted)
PSA：38.33000
Density:1.163±0.06 g/cm3(Predicted)
LogP:2.21090

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylicacidmethylesterhydrochloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride

There total 8 articles about 2-Aza-tricyclo[3.3.1.13,7]decane-5-carboxylic acid Methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 67-56-1
methanol

: 64-18-6
formic acid

: 1448698-97-2
2-azatricyclo[3.3.1.1^3,7]decan-5-ol trifluoroacetate

: 1389264-13-4
methyl 2-azatricyclo[3.3.1.1³'⁷]decane-5-carboxylate

Guidance literature:: formic acid; 2-azatricyclo[3.3.1.1^3,7]decan-5-ol trifluoroacetate; With sulfuric acid; sulfur trioxide; at 60 ℃; for 2h;

methanol; at 0 - 20 ℃;

Reference yield:

: 2-aza-tricyclo[3.3.1.1.^3.7]decane-2-carboxylic acid methyl ester

: 1389264-13-4
methyl 2-azatricyclo[3.3.1.1³'⁷]decane-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 1,4-dioxane / 8 h / 90 °C / Sealed tube

2.1: nitric acid; sulfuric acid / 12 h / 80 °C

2.2: 12 h / 0 - 20 °C

3.1: dichloromethane / 4 h / 0 °C

4.1: sulfuric acid; sulfur trioxide / 2 h / 60 °C

4.2: 0 - 20 °C

With hydrogenchloride; sulfuric acid; sulfur trioxide; nitric acid; In 1,4-dioxane; dichloromethane;

Reference yield:

: 3015-17-6
methyl 2-azatricyclo[3.3.1.1^3,7]decane hydrochloride

: 1389264-13-4
methyl 2-azatricyclo[3.3.1.1³'⁷]decane-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid; sulfuric acid / 12 h / 80 °C

1.2: 12 h / 0 - 20 °C

2.1: dichloromethane / 4 h / 0 °C

3.1: sulfuric acid; sulfur trioxide / 2 h / 60 °C

3.2: 0 - 20 °C

With sulfuric acid; sulfur trioxide; nitric acid; In dichloromethane;