Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester

Base Information

Chemical Name:Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester
CAS No.:1345847-73-5
Molecular Formula:C12H13NO3
Molecular Weight:219.24
Hs Code.:
Mol file:1345847-73-5.mol

Synonyms:Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester;methyl 1-(phenylcarbamoyl)cyclopropanecarboxylate

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Chemical Property of Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester

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Technology Process of Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester

There total 2 articles about Cyclopropanecarboxylic acid,1-[(phenylaMino)carbonyl]-,Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 113020-21-6
1,1-cyclopropanedicarboxylic acid monomethyl ester

: 62-53-3
aniline

: 1345847-73-5
methyl 1-(phenylcarbamoyl)cyclopropanecarboxylate

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield: 86.0%

: 67-56-1
methanol

: 937733-22-7
1-acetyl-N-phenylcyclopropane-1-carboxamide

: 1345847-73-5
methyl 1-(phenylcarbamoyl)cyclopropanecarboxylate

Guidance literature:: With iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1055/s-0031-1289693

Reference yield: 85.0%

: 1345847-73-5
methyl 1-(phenylcarbamoyl)cyclopropanecarboxylate

: 145591-80-6
1-(phenylcarbamoyl)cyclopropane-1-carboxylic acid

Guidance literature:: methyl 1-(phenylcarbamoyl)cyclopropanecarboxylate; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h;

With hydrogenchloride; pH=4; Cooling with ice;