3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI)

Base Information

• Chemical Name: 3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI)
• CAS No.: 172821-14-6
• Molecular Formula: C₉H₁₄O₂
• Molecular Weight: 154.209
• Mol file: 172821-14-6.mol

Synonyms:3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI)

Chemical Property of 3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI)

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Technology Process of 3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI)

There total 15 articles about 3-Cyclohexene-1-carboxylicacid,4,6-dimethyl-,(1S-trans)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(4S)-3-((4'S,5'S)-1',5'-dimethylcyclohexene-4'-carbonyl)-4-(phenylmethyl)-2-oxazolidinone (90719-43-0) → (1S,6S)-4,6-dimethyl-cyclohex-3-enecarboxylic acid (172821-14-6,30631-10-8,58396-02-4)

Guidance literature:

With lithium hydroxide monohydrate; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; Cooling with ice;

Reference yield: 78.0%

(4S)-4-benzyl-3-((6S)-4,6-dimethylcyclohex-3-ene-1-carbonyl)oxazolidin-2-one → (6S)-4,6-dimethyl-cyclohex-3-enecarboxylic acid (172821-14-6,30631-10-8,58396-02-4)

Guidance literature:

With lithium hydroxide monohydrate; water; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 16h; Cooling with ice;

Reference yield: 65.0%

3-[(4',6'-dimethylcyclohex-3'-ene-1'-yl)carbonyl]-oxazolidin-2-one → trans-(4',6'-dimethylcyclohex-3'-ene-1'-yl)-carboxylic acid (172821-14-6,30631-10-8,58396-02-4)

Guidance literature:

With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 15h;

DOI:10.1039/b605244d

upstream raw materials:

2-butenoic acid

hydroquinone

isoprene

(E)-but-2-enoic acid

Downstream raw materials:

(1S,6S)-4,6-dimethylcyclohex-3-ene-carboxylic acid [5-(3,3-dimethylbut-1-ynyl)thiophen-3-yl]-(1,4-dioxa-spiro[4.5]dec-8-yl)amide

(1S,6S)-4,6-dimethylcyclohex-3-enecarboxylic acid [5-(3,3-dimethylbut-1-ynyl)thiophen-3-yl]-(4-oxocyclohexyl)amide

methyl 5-(3,3-dimethylbut-1-ynyl)-3-((1R,6R)-N-isopropyl-4,6-dimethylcyclohex-3-enecarboxamido)thiophene-2-carboxylate

5-(3,3-dimethylbut-1-ynyl)-3-(( 1R,6R)-N-isopropyl-4,6-dimethylcyclohex-3-enecarboxamido)thiophene-2-carboxylic acid

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