1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1)

Base Information

Chemical Name:1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1)
CAS No.:15613-15-7
Molecular Formula:C₁₂H₁₀CuN₄O₄
Molecular Weight:337.782
Hs Code.:
Mol file:15613-15-7.mol

Synonyms:Copper,bis(N-hydroxy-N-nitrosobenzenaminato-O,O')-; Copper,bis(N-nitroso-N-phenylhydroxylaminato)- (6CI,7CI,8CI); Benzenamine,N-hydroxy-N-nitroso-, copper complex;Bis(N-nitroso-N-phenylhydroxylaminato)copper;Bis(N-nitroso-N-phenylhydroxylaminato)copper(II); Bis(cupferronato)copper; NSC56757; NSC 7703

Suppliers and Price of 1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1)

Chemical Property:

Vapor Pressure:0.0169mmHg at 25°C
Boiling Point:243.8°Cat760mmHg
Flash Point:101.3°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1)

There total 3 articles about 1-hydroxy-2-oxo-1-phenylhydrazine - copper (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: copper(II) oxide

: 15613-15-7,52079-21-7
Cu(C₆H₅N₂O₂)2

Guidance literature:: With Mg; NO; phenyl halide; In diethyl ether; water; slow addn. of phenylhalide to Mg in ether; refluxing (1h); cooling; addn. of NO into evacuated flask; stirring; removal of solvent; dissolving of dried NO-Grignard in H2O; addn. of aq. H2SO4; extn. into ether; stirring of extract with CuO for several h;; suspn. was stored overnight; excess of CuO was filtered off and washed with acetone; filtrate and acetone washings were combined and evapd. to dryness; recrystn. from methylated spirits; dried under vac.;;
DOI:10.1016/S0277-5387(00)80898-0

Reference yield:

: cupferron

: 7758-99-8
copper(II) sulfate

: 15613-15-7,52079-21-7
Cu(C₆H₅N₂O₂)2

Guidance literature:: In water;

Reference yield:

: cupferron

: 6046-93-1
copper(II) acetate monohydrate

: 52079-21-7,15613-15-7
bis(cupferronato)copper(II)

Guidance literature:: In methanol; acetonitrile; Cu(CH3COO)2 in MeOH addn. to cupferron in CH3CN, refluxing for 4 d;
DOI:10.1107/S0108270195002770