4-Methylumbelliferyl beta-glucuronide

Base Information

• Chemical Name: 4-Methylumbelliferyl beta-glucuronide
• CAS No.: 84434-84-4
• Molecular Formula: C₁₆H₁₆O₉
• Molecular Weight: 352.298
• Mol file: 84434-84-4.mol

Synonyms:4-Methylumbelliferyl beta-glucuronide

Chemical Property of 4-Methylumbelliferyl beta-glucuronide

Chemical Property:

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Technology Process of 4-Methylumbelliferyl beta-glucuronide

There total 39 articles about 4-Methylumbelliferyl beta-glucuronide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

methyl (4′-methylumbelliferyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)urinate (101014-65-7) → 4-methylumbelliferyl-β-D-glucuronide (6160-80-1,84434-84-4)

Guidance literature:

With water; potassium carbonate; In methanol; dichloromethane; at 0 - 5 ℃; for 12h;

Reference yield: 85.0%

4-methylumbelliferyl-2,3,4-tri-O-acetyl-β-D-glucopyranosiduronic acid (937018-37-6) → 4-methylumbelliferyl-β-D-glucuronide (6160-80-1,84434-84-4)

Guidance literature:

With barium methoxide; In methanol; at 0 - 5 ℃; for 24h;

DOI:10.1055/s-2007-967972

Reference yield: 83.2%

4-methylcoumarin-7-yl-α-L-iduronic acid methyl ester (128095-52-3) → 4-methylcoumarin-7-yl α-L-idopyranosiduronic acid (66966-09-4,84434-84-4)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; at -10 ℃; for 2h;

upstream raw materials:

4-methylumbelliferyl β-D-glucopyranoside

7-hydroxy-4-methyl-chromen-2-one

UDP-glucuronic acid

methyl 4-methylcoumarin-7-yl-β-D-glucopyranuronate

Downstream raw materials:

methyl 4-methylcoumarin-7-yl-β-D-glucopyranuronate

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