2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester

Base Information

Chemical Name:2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester
CAS No.:1177266-41-9
Molecular Formula:C19H28N2O2
Molecular Weight:316.444
Hs Code.:
Mol file:1177266-41-9.mol

Synonyms:2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester

Suppliers and Price of 2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of 2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester

There total 2 articles about 2,7-Diazaspiro[4.4]nonane-2-carboxylic acid, 7-(phenylMethyl)-, 1,1-diMethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 885275-27-4
2-benzyl 2,7-diaza-spiro-[4.4]nonane

: 24424-99-5
di-tert-butyl dicarbonate

: 1177266-41-9
tert-butyl 7-benzyl-2,7-diazaspiro[4.4]nonane-2-carboxylate

Guidance literature:: In dichloromethane;
DOI:10.1016/j.bmcl.2009.01.099

Reference yield: 40.0%

: 2306252-57-1
2,7-diazaspiro[4.4]-nonane-2-carboxylic acid tert-butyl ester

: 100-52-7
benzaldehyde

: 1177266-41-9
tert-butyl 7-benzyl-2,7-diazaspiro[4.4]nonane-2-carboxylate

Guidance literature:: 2,7-diazaspiro[4.4]-nonane-2-carboxylic acid tert-butyl ester; benzaldehyde; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 12h;