p-Methoxy-N,N-dimethylbenzamide

Base Information

• Chemical Name: p-Methoxy-N,N-dimethylbenzamide
• CAS No.: 7291-00-1
• Molecular Formula: C10H13NO2
• Molecular Weight: 179.219
• Mol file: 7291-00-1.mol

Synonyms:N,n-dimethyl-4-methoxybenzamide;N,N-Dimethyl-p-anisamide;p-MeOC6H4CONMe2;4-methoxy-N,N-dimethyl-benzamide;4-MeOC6H4CONMe2;N,N-Dimethyl-p-methoxybenzamide;N,N-dimethylanisamide;

Chemical Property of p-Methoxy-N,N-dimethylbenzamide

Chemical Property:

• Vapor Pressure: 0.000438mmHg at 25°C
• Refractive Index: 1.5150 (estimate)
• Boiling Point: 315.4°Cat760mmHg
• Flash Point: 144.6°C
• PSA: 29.54000
• Density: 1.062g/cm³
• LogP: 1.39700

Purity/Quality:

99% ^*data from raw suppliers

4-methoxy-N,N-dimethylbenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Methoxy-N,N-dimethylbenzamide

There total 53 articles about p-Methoxy-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

para-iodoanisole (696-62-8) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N,N-dimethyl-4-methoxybenzamide (7291-00-1)

Guidance literature:

With sodium methylate; nickel diacetate; In 1,4-dioxane; at 110 ℃;

DOI:10.1021/ol702058e

Reference yield: 98.0%

dimethyl amine (124-40-3) + 4-Methoxybenzyl alcohol (105-13-5) → N,N-dimethyl-4-methoxybenzamide (7291-00-1)

Guidance literature:

With oxygen; sodium hydroxide; In water; at 25 ℃; for 24h;

DOI:10.1016/j.tetlet.2013.10.133

Reference yield: 90.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 4-Methoxybenzyl alcohol (105-13-5) → N,N-dimethyl-4-methoxybenzamide (7291-00-1)

Guidance literature:

With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In 1,1,2-trichloroethane; water; at 90 ℃; for 12h;

DOI:10.1016/j.tetlet.2012.09.039

upstream raw materials:

4-methoxy-benzoyl chloride

dimethyl amine

Dimethylamino-(4-methoxy-phenyl)-trimethylsilanyloxy-acetonitrile

C₁₁H₁₆NO₅P

Downstream raw materials:

N,N-dimethyl-4-methoxylbenzylamine

3-(4-methoxy-phenyl)-5,6-dihydro-4H-cyclopenta[c]isoxazole

1-(4-methoxy-phenyl)-3-phenyl-propynone

[(4-Methoxy-phenyl)-trichlorosilanyl-methyl]-dimethyl-amine