2-(3,5-diMethylphenyl)benzonitrile

Base Information

Chemical Name:2-(3,5-diMethylphenyl)benzonitrile
CAS No.:1355247-46-9
Molecular Formula:C₁₅H₁₃N
Molecular Weight:207.275
Hs Code.:2926909090
Mol file:1355247-46-9.mol

Synonyms:2-(3,5-diMethylphenyl)benzonitrile

Suppliers and Price of 2-(3,5-diMethylphenyl)benzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(3,5-dimethylphenyl)benzonitrile
500mg
$ 70.00

Crysdot
2-(3,5-dimethylphenyl)benzonitrile 95+%
25g
$ 565.00

Total 3 raw suppliers

Chemical Property of 2-(3,5-diMethylphenyl)benzonitrile

Chemical Property:

PSA：23.79000
LogP:3.84208

Purity/Quality:

99% ^*data from raw suppliers

2-(3,5-dimethylphenyl)benzonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(3,5-diMethylphenyl)benzonitrile

There total 3 articles about 2-(3,5-diMethylphenyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22445-41-6
3,5-dimethylphenyl iodide

: 172732-52-4
o-cyanophenylboronic acid-1,3-propylene glycol ester

: 1355247-46-9
3',5'-dimethyl-[1,1'-biphenyl]-2-carbonitrile

Guidance literature:: With tripotassium phosphate "n" hydrate; Pd(PPh₃)₂Cl₂; In toluene; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol401063w

Reference yield:

: 138642-62-3
2-Cyanophenylboronic acid

: 1355247-46-9
3',5'-dimethyl-[1,1'-biphenyl]-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2 h / 110 °C

2: Pd(PPh₃)₂Cl₂; tripotassium phosphate "n" hydrate / toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

With tripotassium phosphate "n" hydrate; Pd(PPh₃)₂Cl₂; In toluene;
DOI:10.1021/ol401063w

Reference yield:

: 556-96-7
5-bromo-1,3-xylene

: 100-47-0
benzonitrile

: 935552-89-9
3',5'-dimethyl-[1,1'-biphenyl]-4-carbonitrile

: 1355247-46-9
3',5'-dimethyl-[1,1'-biphenyl]-2-carbonitrile

: 713079-19-7
3-carbonitrile-3',5'-dimethyl-1,1'-biphenyl

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); potassium carbonate; Trimethylacetic acid; In N,N-dimethyl acetamide; at 120 ℃; for 3h; Overall yield = 72 percentChromat.;
DOI:10.1039/d0sc05414c