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2-Cyanophenylboronic acid -1,3-propanediol ester
Cas No: 172732-52-4
No Data 100 Gram 5 Metric Ton/Month Hebei Maison Chemical Co.,Ltd Contact Supplier
2-(1,3,2-DIOXABORINAN-2-YL)BENZONITRILE
Cas No: 172732-52-4
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
2-(1,3,2-DIOXABOROLAN-2-YL)BENZONITRILE
Cas No: 172732-52-4
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
2-Cyanophenylboronic acid 1,3-propanediol ester
Cas No: 172732-52-4
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2-(1,3,2-Dioxaborinan-2-yl)-benzonitrile
Cas No: 172732-52-4
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
2-Cyanophenylboronic acid 1,3-propanediol ester
Cas No: 172732-52-4
USD $ 23.0-23.0 / Kilogram 1 Kilogram 200 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
172732-52-4 2-(1,3,2-DIOXABOROLAN-2-YL)BENZONITRILE
Cas No: 172732-52-4
USD $ 1000.0-1000.0 / Kilogram 1 Kilogram 1 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
2-Cyanophenylboronic acid-1,3-propanediol cyclic ester
Cas No: 172732-52-4
No Data 1 Metric Ton 100 Metric Ton/Day Shanghai AngewChem Co., Ltd. Contact Supplier
Pharmaceutical Grade CAS 172732-52-4 with competitive price
Cas No: 172732-52-4
USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support 2-(1,3,2-Dioxaborinan-2-yl)benzonitrile CAS 172732-52-4
Cas No: 172732-52-4
No Data 1 Gram 3 Metric Ton/Month Shaanxi BLOOM TECH Co.,Ltd Contact Supplier

172732-52-4 Usage

Chemical Properties

White powder
InChI:InChI=1/C10H10BNO2/c12-8-9-4-1-2-5-10(9)11-13-6-3-7-14-11/h1-2,4-5H,3,6-7H2

172732-52-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (653934)  2-Cyanophenylboronicacid1,3-propanediolester  96% 172732-52-4 653934-1G 1,788.93CNY Detail
TCI America (C2993)  2-Cyanophenylboronic Acid 1,3-Propanediol Ester  >97.0%(GC) 172732-52-4 5g 2,360.00CNY Detail
TCI America (C2993)  2-Cyanophenylboronic Acid 1,3-Propanediol Ester  >97.0%(GC) 172732-52-4 1g 680.00CNY Detail

172732-52-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-(1,3,2-Dioxaborinan-2-yl)benzonitrile

1.2 Other means of identification

Product number -
Other names 2-(1,3,2-dioxaborinan-2-yl)benzonitrile

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:172732-52-4 SDS

172732-52-4Synthetic route

2-Cyanophenylboronic acid
138642-62-3

2-Cyanophenylboronic acid

trimethyleneglycol
504-63-2

trimethyleneglycol

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

Conditions
ConditionsYield
at 20℃; for 1h;82.4%
In dichloromethane57.2%
In dichloromethane for 20h;57.2%
o-cyanobromobenzene
2042-37-7

o-cyanobromobenzene

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: toluene / 0.5 h / 0 - 5 °C / Inert atmosphere
1.2: 1.5 h / 0 - 5 °C
1.3: 0.75 h / 0 - 25 °C
2.1: hydrogenchloride / water / 0.5 h / 0 - 25 °C
3.1: toluene; tetrahydrofuran; Isopropyl acetate / 2 h / 20 - 25 °C
View Scheme
benzonitrile
100-47-0

benzonitrile

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium chloride; n-butyllithium / tetrahydrofuran; hexane / -10 °C / Inert atmosphere
1.2: -50 °C / Inert atmosphere
1.3: Inert atmosphere
2.1: 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: 2,2,6,6-tetramethyl-piperidine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 3 h / -50 - -10 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: 1 h / 20 °C
View Scheme
2-bromoanisole
578-57-4

2-bromoanisole

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2'-methoxy-[1,1'-biphenyl]-2-carbonitrile

2'-methoxy-[1,1'-biphenyl]-2-carbonitrile

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene for 1h; Heating;99%
benzoimidazole
51-17-2

benzoimidazole

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

A

salicylonitrile
611-20-1

salicylonitrile

B

benzonitrile
100-47-0

benzonitrile

C

2-(1H-benzo[d]imidazol-1-yl)benzonitrile
25699-93-8

2-(1H-benzo[d]imidazol-1-yl)benzonitrile

Conditions
ConditionsYield
With pyridine; water; copper diacetate In N,N-dimethyl-formamide at 30℃; for 24h; Kinetics; Product distribution; Further Variations:; Reaction partners; amount of water;A n/a
B n/a
C 93%
2-Bromo-m-xylene
576-22-7

2-Bromo-m-xylene

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2',6'-dimethyl-[1,1'-biphenyl]-2-carbonitrile

2',6'-dimethyl-[1,1'-biphenyl]-2-carbonitrile

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene for 1h; Heating;92%
tert-butyl N-(3-(3-iodo-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

tert-butyl N-(3-(3-iodo-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

tert-butyl N-(3-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

tert-butyl N-(3-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110℃; for 2h; Inert atmosphere;90%
tert-butyl N-(3-(3-iodo-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

tert-butyl N-(3-(3-iodo-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(1,3,2-dioxaboran-2-yl)benzonitrile

2-(1,3,2-dioxaboran-2-yl)benzonitrile

tert-butyl N-(3-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

tert-butyl N-(3-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-1-yl)phenyl)carbamate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110℃; for 2h; Inert atmosphere;90%
(E)-2-methylbut-2-enoyl chloride
35660-94-7

(E)-2-methylbut-2-enoyl chloride

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-[(E)-2-methylbut-2-enoyl]benzonitrile

2-[(E)-2-methylbut-2-enoyl]benzonitrile

Conditions
ConditionsYield
With potassium phosphate; bis-triphenylphosphine-palladium(II) chloride In toluene at 80℃; for 4h;89%
3-iodo-1-(3-dimethylaminophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

3-iodo-1-(3-dimethylaminophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(1-(3-dimethylaminophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

2-(1-(3-dimethylaminophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 115℃; for 0.333333h; Inert atmosphere;89%
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate89%
o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

1-{3-bromo-4-chloro-5-[1-(R)-fluoropropyl]}phenylpiperazine
172732-49-9

1-{3-bromo-4-chloro-5-[1-(R)-fluoropropyl]}phenylpiperazine

1-{3-(2-cyanophenyl)-4-chloro-5-[1-(R)-fluoropropyl]}phenyl piperazine

1-{3-(2-cyanophenyl)-4-chloro-5-[1-(R)-fluoropropyl]}phenyl piperazine

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene Product distribution; Further Variations:; Reagents;87%
With trans-bis(triphenylphosphine)palladium dichloride; tripotassium phosphate "n" hydrate In toluene at 20℃; for 1h; Suzuki-Miyaura Coupling; Reflux; Inert atmosphere; Large scale;
3-bromo-5-(2-pyridyl)-1-(3-pyridyl)-1,2-dihydropyridin-2-one

3-bromo-5-(2-pyridyl)-1-(3-pyridyl)-1,2-dihydropyridin-2-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

3-(2-cyanophenyl)-5-(pyridin-2-yl)-1-(pyridin-3-yl)-1,2-dihydropyridin-2-one

3-(2-cyanophenyl)-5-(pyridin-2-yl)-1-(pyridin-3-yl)-1,2-dihydropyridin-2-one

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 120℃; for 1h; Suzuki-Miyaura Coupling;84%
potassium phosphate

potassium phosphate

1-(2-trimethylsilyloxyethyl)-4-[3-bromo-4-chloro-5-(1-fluoropropyl)]phenylpiperazine
172732-42-2

1-(2-trimethylsilyloxyethyl)-4-[3-bromo-4-chloro-5-(1-fluoropropyl)]phenylpiperazine

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

1-(2-hydroxyethyl)-4-[3-(2-cyanophenyl)-4-chloro-5-(1-fluoropropyl)]phenylpiperazine hydrochloride
172732-18-2

1-(2-hydroxyethyl)-4-[3-(2-cyanophenyl)-4-chloro-5-(1-fluoropropyl)]phenylpiperazine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; tetrakis(triphenylphosphine)palladium (0) In ethanol; water; N,N-dimethyl-formamide83.9%
3-acetylamino-1-(4-iodo-phenyl)-1H-pyrazole-4-carboxylicacid ethyl ester
1335105-20-8

3-acetylamino-1-(4-iodo-phenyl)-1H-pyrazole-4-carboxylicacid ethyl ester

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

3-acetylamino-1-(2'-cyano-biphenyl-4-yl)-1H-pyrazole-4-carboxylic acid ethyl ester
1335105-40-2

3-acetylamino-1-(2'-cyano-biphenyl-4-yl)-1H-pyrazole-4-carboxylic acid ethyl ester

Conditions
ConditionsYield
With potassium phosphate; PdCl2(dppf) In toluene for 2h; Suzuki reaction; Reflux;83%
iodobenzene
591-50-4

iodobenzene

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

biphenyl-2-carbonitrile
24973-49-7

biphenyl-2-carbonitrile

Conditions
ConditionsYield
With tripotassium phosphate "n" hydrate; Pd(PPh3)2Cl2 In toluene at 100℃; for 12h; Schlenk technique; Inert atmosphere;77%
1-bromo-2,5-dimethoxybenzene
25245-34-5

1-bromo-2,5-dimethoxybenzene

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2',5'-dimethoxy-[1,1'-biphenyl]-2-carbonitrile
75860-41-2

2',5'-dimethoxy-[1,1'-biphenyl]-2-carbonitrile

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene for 1h; Heating;76%
C16H12BrN3O2
1415212-92-8

C16H12BrN3O2

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(1-(6-methoxypyridin-3-yl)-2-oxo-5-(pyridin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

2-(1-(6-methoxypyridin-3-yl)-2-oxo-5-(pyridin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110 - 120℃; for 24h; Inert atmosphere;75%
3-bromo-5-(2-pyridyl)-1-phenyl-1,2-dihydropyridine-2-one
381248-06-2

3-bromo-5-(2-pyridyl)-1-phenyl-1,2-dihydropyridine-2-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

[14C]-Perampanel
380917-97-5

[14C]-Perampanel

Conditions
ConditionsYield
With caesium carbonate; palladium dichloride In N,N-dimethyl-formamide at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere;73%
Stage #1: 3-bromo-5-(2-pyridyl)-1-phenyl-1,2-dihydropyridine-2-one; o-cyanophenylboronic acid-1,3-propylene glycol ester With copper(l) iodide; potassium carbonate; palladium diacetate; triphenylphosphine In 1,2-dimethoxyethane at 70℃; for 4.5h; Heating / reflux;
Stage #2: With ammonia In water at 60℃; for 0.883333h;
With potassium carbonate; palladium diacetate; copper(l) iodide; triphenylphosphine In 1,2-dimethoxyethane at 70℃; for 4.5h; Heating / reflux;
With copper(l) iodide; potassium carbonate; palladium diacetate; triphenylphosphine In 1,2-dimethoxyethane at 70℃; for 4.5h; Heating / reflux;
With tetrakis(triphenylphosphine) palladium(0); triethylamine In dichloromethane at 25 - 30℃; for 12h; Reagent/catalyst; Temperature; Solvent;
C17H10BrN3O
1415212-90-6

C17H10BrN3O

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

C24H14N4O
380919-04-0

C24H14N4O

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110 - 120℃; for 24h; Inert atmosphere;73%
potassium phosphate

potassium phosphate

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

1-{3-bromo-4-chloro-5-[1-(R)-fluoropropyl]}phenylpiperazine
172732-49-9

1-{3-bromo-4-chloro-5-[1-(R)-fluoropropyl]}phenylpiperazine

1-{3-(2-cyanophenyl)-4-chloro-5-[1-(R)-fluoropropyl]}phenyl piperazine

1-{3-(2-cyanophenyl)-4-chloro-5-[1-(R)-fluoropropyl]}phenyl piperazine

Conditions
ConditionsYield
tetrakis(triphenylphosphine) palladium(0) In water; ethyl acetate; N,N-dimethyl-formamide71%
5-[acetyl-(4-iodo-phenyl)-amino]-1-butyl-1H-pyrazole-4-carboxylic acid ethyl ester
1335105-43-5

5-[acetyl-(4-iodo-phenyl)-amino]-1-butyl-1H-pyrazole-4-carboxylic acid ethyl ester

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

5-[acetyl-(2'-cyano-biphenyl-4-yl)-amino]-1-butyl-1H-pyrazole-4-carboxylic acid ethyl ester
1335105-44-6

5-[acetyl-(2'-cyano-biphenyl-4-yl)-amino]-1-butyl-1H-pyrazole-4-carboxylic acid ethyl ester

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In water; toluene for 1.5h; Suzuki reaction; Reflux;71%
benzoyl chloride
98-88-4

benzoyl chloride

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-cyanobenzophenone
37774-78-0

2-cyanobenzophenone

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene at 110℃; for 4h; Product distribution; Further Variations:; Reagents; Solvents; Suzuki-Miyaura coupling recation;70%
tert-butyl (2-fluoro-5-(3-iodo-2-oxo-5-(pyrimidin-2-yl)pyridin-1(2H)-yl)phenyl)carbamate

tert-butyl (2-fluoro-5-(3-iodo-2-oxo-5-(pyrimidin-2-yl)pyridin-1(2H)-yl)phenyl)carbamate

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

tert-butyl (5-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)pyridin-1(2H)-yl)-2-fluorophenyl)carbamate

tert-butyl (5-(3-(2-cyanophenyl)-2-oxo-5-(pyrimidin-2-yl)pyridin-1(2H)-yl)-2-fluorophenyl)carbamate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110℃; for 1h; Inert atmosphere;68%
5-(2-pyridyl)-3-bromo-2-methoxypyridine
381248-05-1

5-(2-pyridyl)-3-bromo-2-methoxypyridine

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

3-(2-cyanophenyl)-5-(2-pyridyl)-2-methoxypyridine

3-(2-cyanophenyl)-5-(2-pyridyl)-2-methoxypyridine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 140℃; for 5h; Inert atmosphere;66%
2-bromo-4-butylaniline
51605-98-2

2-bromo-4-butylaniline

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(n-butyl)-6-aminophenanthridine
946147-28-0

2-(n-butyl)-6-aminophenanthridine

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine)palladium (0) In ethanol; toluene65.9%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 38h; Reflux; Inert atmosphere;65.9%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 38h; Reflux; Inert atmosphere;65.9%
3-bromo-1-(3-fluorophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

3-bromo-1-(3-fluorophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(1-(3-fluorophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

2-(1-(3-fluorophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; Inert atmosphere;60%
3-iodo-1-(3-fluorophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

3-iodo-1-(3-fluorophenyl)-5-(pyrimidin-2-yl)pyridin-2(1H)-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(1-(3-fluorophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

2-(1-(3-fluorophenyl)-2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate60%
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide Suzuki-Miyaura Coupling;28%
5-bromo-1-phenyl-3-iodo-1,2-dihydropyridin-2-one

5-bromo-1-phenyl-3-iodo-1,2-dihydropyridin-2-one

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

5-bromo-3-(2-cyanophenyl)-1-phenyl-1,2-dihydropyridin-2-one
381233-77-8

5-bromo-3-(2-cyanophenyl)-1-phenyl-1,2-dihydropyridin-2-one

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 80℃; for 2h; Inert atmosphere;52%
C15H9BrFN3O
1415212-89-3

C15H9BrFN3O

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

3-(2-cyanophenyl)-5-(pyridin-2-yl)-1-(2-fluoropyridin-5-yl)-1,2-dihydropyridin-2-one

3-(2-cyanophenyl)-5-(pyridin-2-yl)-1-(2-fluoropyridin-5-yl)-1,2-dihydropyridin-2-one

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110 - 120℃; for 24h; Inert atmosphere;42%
tert-butyl 3-iodo-2-oxo-5-(pyrimidin-2-yl)pyridine-1(2H)-carboxylate

tert-butyl 3-iodo-2-oxo-5-(pyrimidin-2-yl)pyridine-1(2H)-carboxylate

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

2-(2-oxo-5-(pyrimidin-2-yl)-1,2-dihydropyridin-3-yl)benzonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In N,N-dimethyl-formamide at 110℃; Inert atmosphere;41%
2-bromo-4-n-hexylaniline
946147-25-7

2-bromo-4-n-hexylaniline

o-cyanophenylboronic acid-1,3-propylene glycol ester
172732-52-4

o-cyanophenylboronic acid-1,3-propylene glycol ester

2-(n-hexyl)-6-aminophenanthridine

2-(n-hexyl)-6-aminophenanthridine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 20h; Reflux; Inert atmosphere;39.8%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 20h; Reflux; Inert atmosphere;39.8%

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