2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine

Base Information

Chemical Name:2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine
CAS No.:65936-26-7
Molecular Formula:C9H8Cl2N4O2
Molecular Weight:275.094
Hs Code.:
ChEMBL ID:CHEMBL21734
DSSTox Substance ID:DTXSID30879706
Nikkaji Number:J420.196E
Wikidata:Q82861814

Synonyms:CHEMBL21734;65936-26-7;SCHEMBL8763532;DTXSID30879706;JZZSKQYBVLLLKN-UHFFFAOYSA-N;BDBM50226860;2-(26-DICL-4-NO2-PHIMINO)IMIDAZOLIDN;2-[(2,6-dichloro-4-nitrophenyl)imino]imidazolidine

Suppliers and Price of 2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine

Chemical Property:

PSA：82.24000
LogP:3.26270
XLogP3:2.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:274.0024309
Heavy Atom Count:17
Complexity:321

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CN=C(N1)NC2=C(C=C(C=C2Cl)[N+](=O)[O-])Cl

Technology Process of 2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine

There total 8 articles about 2-[(2,6-Dichloro-4-nitrophenyl)imino]imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.4%

: 73218-65-2
(2,6-dichloro-4-nitrophenyl)carbonimidic dichloride

: 107-15-3,85404-18-8
ethylenediamine

: 65936-26-7
2-(2',6'-dichloro-4'-nitroanilino)-2-imidazoline

Guidance literature:: With triethylamine; In ethyl acetate; at 5 ℃; for 6h;

Reference yield: 62.0%

: 73218-65-2
(2,6-dichloro-4-nitrophenyl)carbonimidic dichloride

: 107-15-3,85404-18-8
ethylenediamine

: 65936-26-7,741202-17-5
p-Nitroclonidine

Guidance literature:: ethylenediamine; With triethylamine; In tetrahydrofuran; for 0.25h; Cooling with ice;

(2,6-dichloro-4-nitrophenyl)carbonimidic dichloride; In tetrahydrofuran; at 5 - 20 ℃; for 6.5h;
DOI:10.1080/00304948.2016.1206429

Reference yield:

: 99-30-9
4-nitro-2,6-dichloroaniline

: 65936-26-7,741202-17-5
p-Nitroclonidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 0.33 h / 55 - 60 °C

1.2: 6.33 h / 55 °C

2.1: sulfuryl dichloride; thionyl chloride / 60 °C

3.1: triethylamine / tetrahydrofuran / 0.25 h / Cooling with ice

3.2: 6.5 h / 5 - 20 °C

With thionyl chloride; sulfuryl dichloride; acetic anhydride; triethylamine; In tetrahydrofuran;
DOI:10.1080/00304948.2016.1206429