2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

Base Information

Chemical Name:2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine
CAS No.:108294-56-0
Molecular Formula:C₁₃H₁₆Cl₂N₆
Molecular Weight:327.216
Hs Code.:

Synonyms:2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

Suppliers and Price of 2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

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Technology Process of 2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

There total 3 articles about 2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73218-65-2
(2,6-dichloro-4-nitrophenyl)carbonimidic dichloride

: 108294-56-0
2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / Et₃N / ethyl acetate / 3 h

2: 77 percent / Fe, aq. HCl / ethanol / 3 h / Heating

3: 1.) NaNO₂, aq. H₂SO₄, 2.) aq. KOH / 1.) 0 deg C, 15 min, 2.) from 0 deg C to RT, 15 min

With hydrogenchloride; potassium hydroxide; sulfuric acid; iron; triethylamine; sodium nitrite; In ethanol; ethyl acetate;
DOI:10.1021/jm00390a021

Reference yield:

: 65936-26-7
2-(2',6'-dichloro-4'-nitroanilino)-2-imidazoline

: 108294-56-0
2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Fe, aq. HCl / ethanol / 3 h / Heating

2: 1.) NaNO₂, aq. H₂SO₄, 2.) aq. KOH / 1.) 0 deg C, 15 min, 2.) from 0 deg C to RT, 15 min

With hydrogenchloride; potassium hydroxide; sulfuric acid; iron; sodium nitrite; In ethanol;
DOI:10.1021/jm00390a021

Reference yield:

: 123-75-1
pyrrolidine

: 66711-21-5
p-aminoclonidine

: 108294-56-0
2-({2,6-dichloro-4-[3,3-(1,4-butanediyl)triazeno]phenyl}imino)imidazolidine

Guidance literature:: With potassium hydroxide; sulfuric acid; sodium nitrite; Yield given. Multistep reaction; 1.) 0 deg C, 15 min, 2.) from 0 deg C to RT, 15 min;
DOI:10.1021/jm00390a021