ethyl 2-(cyclopropylamino)acetate

Base Information

• Chemical Name: ethyl 2-(cyclopropylamino)acetate
• CAS No.: 71922-62-8
• Molecular Formula: C7H13NO2
• Molecular Weight: 143.186
• Hs Code.: 2922498590
• Mol file: 71922-62-8.mol

Synonyms:ethyl 2-(cyclopropylamino)acetate;2-(cyclopropylamino)acetic acid ethyl ester;ethyl 2-(cyclopropylamino)ethanoate;ethyl N-cyclopropylglycinate

Chemical Property of ethyl 2-(cyclopropylamino)acetate

Chemical Property:

• PSA: 38.33000
• LogP: 0.69240

Purity/Quality:

99% ^*data from raw suppliers

ethyl2-(cyclopropylamino)acetate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 2-(cyclopropylamino)acetate

There total 2 articles about ethyl 2-(cyclopropylamino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl bromoacetate (105-36-2) + Cyclopropylamine (765-30-0) → [(cyclopropyl)amino]acetic acid ethyl ester (71922-62-8)

Guidance literature:

In ethanol; for 1h;

Reference yield:

diazoacetic acid ethyl ester (623-73-4) + Cyclopropylamine (765-30-0) → [(cyclopropyl)amino]acetic acid ethyl ester (71922-62-8) + N-(2-ethoxy-2-oxoethyl)-N-(cyclopropyl)glycine ethyl ester

Guidance literature:

With octa-2,3,9,10,16,17,23,24-n-butoxyphthalocyaninatoruthenium(II) carbonyl; In dichloromethane; at 40 ℃; for 20h; Time; Catalytic behavior; Inert atmosphere;

DOI:10.1039/d0dt04090h

Reference yield: 96.8%

ethyl trimethoxybenzoyl acetate (3044-56-2) + [(cyclopropyl)amino]acetic acid ethyl ester (71922-62-8) → 1-Cyclopropyl-3-[1-hydroxy-1-(3,4,5-trimethoxy-phenyl)-meth-(Z)-ylidene]-pyrrolidine-2,4-dione

Guidance literature:

ethyl trimethoxybenzoyl acetate; [(cyclopropyl)amino]acetic acid ethyl ester; In xylene; at 125 - 130 ℃; for 20h;

With sodium methylate; In methanol; xylene; at 20 ℃; for 48h;

DOI:10.1021/jf051510l

upstream raw materials:

ethyl bromoacetate

Cyclopropylamine

diazoacetic acid ethyl ester

Downstream raw materials:

L-cyclopropylglycine

3-[4-cyano-2-fluoro-5-(1-cyclopropyl-2,4-dioxoimidazolidin-3-yl)phenyl]-1-methyl-6-trifluoromethyl-1H-pyrimidin-2,4-dione

[cyclopropyl-(4-trifluoromethoxy-benzoyl)-amino]-acetic acid ethyl ester

ethyl 2-(N-cyclopropyl-4-methoxy-2,6-dimethylphenylsulfonamido)acetate

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