1-Boc-4-MethylaMino-3,3-diMethylpiperidine

Base Information

• Chemical Name: 1-Boc-4-MethylaMino-3,3-diMethylpiperidine
• CAS No.: 1242240-00-1
• Molecular Formula: C13H26N2O2
• Molecular Weight: 242.362
• Mol file: 1242240-00-1.mol

Synonyms:tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate

Chemical Property of 1-Boc-4-MethylaMino-3,3-diMethylpiperidine

Chemical Property:

• PSA: 41.57000
• LogP: 2.57020

Purity/Quality:

99%, ^*data from raw suppliers

1-Boc-4-methylamino-3,3-dimethylpiperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Boc-4-MethylaMino-3,3-diMethylpiperidine

There total 1 articles about 1-Boc-4-MethylaMino-3,3-diMethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

methylamine (74-89-5) + tert-butyl 3,3-dimethyl-4-oxopiperidine-1-carboxylate (324769-06-4) → tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate (1242240-00-1)

Guidance literature:

With hydrogen; 5%-palladium/activated carbon; In methanol; at 60 ℃; under 2585.81 Torr;

Reference yield: 82.0%

tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate (1242240-00-1) + 1-(2,3-dichloro-4-methoxyphenyl)ethanamine (1368225-72-2) → C23H35Cl2N3O4 (1394860-39-9)

Guidance literature:

1-(2,3-dichloro-4-methoxyphenyl)ethanamine; With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield: 82.0%

tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate (1242240-00-1) + bis(trichloromethyl) carbonate (32315-10-9) + 1-(2,3-dichloro-4-methoxyphenyl)ethanamine (1368225-72-2) → C23H35Cl2N3O4 (1394860-39-9)

Guidance literature:

bis(trichloromethyl) carbonate; 1-(2,3-dichloro-4-methoxyphenyl)ethanamine; With triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

tert-butyl 3,3-dimethyl-4-(methylamino)piperidine-1-carboxylate; In dichloromethane; at 0 ℃; for 0.5h;

upstream raw materials:

methylamine

tert-butyl 3,3-dimethyl-4-oxopiperidine-1-carboxylate

Downstream raw materials:

C₂₃H₃₅Cl₂N₃O₄

C₁₈H₂₇Cl₂N₃O₂

3-(1-(2,3-dichloro-4-methoxyphenyl)ethyl)-1-methyl-1-(1,3,3-trimethylpiperidin-4-yl)urea

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