p-Anisaldehyde o-nitrophenyl hydrazone

Base Information

• Chemical Name: p-Anisaldehyde o-nitrophenyl hydrazone
• CAS No.: 15941-05-6
• Molecular Formula: C14H13N3O3
• Molecular Weight: 271.27
• Mol file: 15941-05-6.mol

Synonyms:p-Anisaldehyde o-nitrophenyl hydrazone

Chemical Property of p-Anisaldehyde o-nitrophenyl hydrazone

Chemical Property:

• Melting Point: 210 - 212 °C (ethanol)
• PSA: 79.44000
• LogP: 3.64560

Purity/Quality:

99% ^*data from raw suppliers

1-(4-methoxybenzylidene)-2-(2-nitrophenyl)hydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-Anisaldehyde o-nitrophenyl hydrazone

There total 2 articles about p-Anisaldehyde o-nitrophenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(4-methoxyphenylmethylene)malononitrile (2826-26-8) + 1-[2-(2-nitrophenyl)hydrazono]propan-2-ol (1197992-89-4) → 4-methoxybenzaldehyde 2-nitrophenylhydrazone (15941-05-6)

Guidance literature:

With piperidine; In ethanol; Reflux;

DOI:10.1016/j.tetlet.2009.08.037

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + (2-nitrophenyl)hydrazine (3034-19-3) → 4-methoxybenzaldehyde 2-nitrophenylhydrazone (15941-05-6)

Guidance literature:

With acetic acid; at 110 ℃;

DOI:10.1021/acs.orglett.1c03993

Reference yield:

4-methoxybenzaldehyde 2-nitrophenylhydrazone (15941-05-6) → 1,2-Bis-(4-methoxy-phenyl)-2-[(2-nitro-phenyl)-hydrazono]-ethanone

Guidance literature:

With thallium(III) acetate; sodium chloride; In acetic acid; at 50 ℃; Rate constant; Mechanism;

upstream raw materials:

2-(4-methoxyphenylmethylene)malononitrile

1-[2-(2-nitrophenyl)hydrazono]propan-2-ol

4-methoxy-benzaldehyde

(2-nitrophenyl)hydrazine

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