METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE

Base Information

• Chemical Name: METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE
• CAS No.: 893616-55-2
• Molecular Formula: C8H9NO4
• Molecular Weight: 183.16
• Hs Code.: 2933399090
• Mol file: 893616-55-2.mol

Synonyms:METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE;3-pyridinecarboxylic acid, 2,4-dihydroxy-6-Methyl-, Methyl ester

Chemical Property of METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE

Chemical Property:

• PSA: 79.65000
• LogP: 0.58780
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

Methyl2,4-dihydroxy-6-methylnicotinate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE

There total 1 articles about METHYL 2,4-DIHYDROXY-6-METHYLNICOTINATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-aminocrotonate (21731-17-9) + malonic acid dimethyl ester (108-59-8) → C8H9NO4 (893616-55-2)

Guidance literature:

With sodium methylate; In xylene; Heating;

DOI:10.1021/jm070579c

Reference yield: 44.0%

2,4-dihydroxy-6-methyl-3-pyridinecarboxylic acid methyl ester (893616-55-2) + 4-phenoxyanilin (139-59-3) → 4-hydroxy-6-methyl-2-oxo-1,2-dihydro-pyridine-3-carboxylic acid (4-phenoxy-phenyl)-amide

Guidance literature:

In tetrahydrofuran; at 180 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

C8H9NO4 (893616-55-2) → methyl 2,4-dichloro-6-methylpyridine-3-carboxylate (138642-40-7)

Guidance literature:

With N,N-diethylaniline; trichlorophosphate; In xylene;

DOI:10.1021/jm070579c

upstream raw materials:

methyl 3-aminocrotonate

malonic acid dimethyl ester

Downstream raw materials:

methyl 2,4-dichloro-6-methylpyridine-3-carboxylate

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