3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

Base Information

• Chemical Name: 3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate
• CAS No.: 889654-06-2
• Molecular Formula: C15H21BO5
• Molecular Weight: 292.14
• Hs Code.: 2934999090
• Mol file: 889654-06-2.mol

Synonyms:3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate;3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoic acid methyl ester;Methyl 3-Methoxy-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)benzoate;3-Methoxy-5-(methoxycarbonyl)phenylboronic acid, pinacol ester

Chemical Property of 3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

Chemical Property:

• PSA: 53.99000
• LogP: 1.78100
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxy-5-Methoxycarbonylphenylboronicacidpinacolester 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

There total 6 articles about 3-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 3-methoxybenzoate (5368-81-0) + bis(pinacol)diborane (73183-34-3) → 3-methoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzoic acid methyl ester (889654-06-2)

Guidance literature:

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In hexane; at 20 ℃; regioselective reaction;

DOI:10.3987/COM-18-S(F)72

Reference yield: 68.0%

methyl 3-methoxy-5-(trifluoromethanesulfonyloxy)benzoate (916343-75-4) + bis(pinacol)diborane (73183-34-3) → 3-methoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzoic acid methyl ester (889654-06-2)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 20 - 90 ℃; for 16h;

DOI:10.1021/jm200553w

Reference yield: 66.0%

3-bromo-5-methoxy-benzoic acid methyl ester (56709-70-7) + bis(pinacol)diborane (73183-34-3) → 3-methoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzoic acid methyl ester (889654-06-2)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; In 1,4-dioxane; at 20 - 90 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tet.2019.01.003

upstream raw materials:

methyl 3-methoxy-5-(trifluoromethanesulfonyloxy)benzoate

bis(pinacol)diborane

3-hydroxy-5-methoxy-benzoic acid methyl ester

3-bromo-5-hydroxy-benzoic acid

Downstream raw materials:

[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

1-methoxy-3-methoxycarbonyl-9H-carbazole

1-methoxy-3-methylcarbazole

murrayanine

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