[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Base Information

Chemical Name:[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid
CAS No.:1048330-11-5
Molecular Formula:C₉H₁₁BO₅
Molecular Weight:209.994
Hs Code.:9999999999

Synonyms:[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Suppliers and Price of [3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Borono-5-methoxy-benzoicAcid1-MethylEster
100mg
$ 725.00

J&W Pharmlab
3-Methoxy-5-Methoxycarbonylphenylboronicacid 97%
5g
$ 1800.00

Crysdot
(3-Methoxy-5-(methoxycarbonyl)phenyl)boronicacid 95+%
1g
$ 491.00

Alichem
(3-Methoxy-5-(methoxycarbonyl)phenyl)boronicacid
1g
$ 998.00

AK Scientific
[3-Methoxy-5-(methoxycarbonyl)phenyl]boronicacid
1g
$ 1651.00

AK Scientific
[3-Methoxy-5-(methoxycarbonyl)phenyl]boronicacid
250mg
$ 691.00

Total 9 raw suppliers

Chemical Property of [3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Chemical Property:

Boiling Point:408.3±55.0 °C(Predicted)
Density:1.26±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

3-Borono-5-methoxy-benzoicAcid1-MethylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 3-Borono-5-methoxy-benzoic acid,1-methyl ester

Technology Process of [3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

There total 3 articles about [3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 889654-06-2
3-methoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzoic acid methyl ester

: 1048330-11-5
[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Guidance literature:: With sodium periodate; ammonium acetate; In water; acetone; at 20 ℃;
DOI:10.1021/jm800222k

Reference yield:

: 916343-75-4
methyl 3-methoxy-5-(trifluoromethanesulfonyloxy)benzoate

: 1048330-11-5
[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; potassium acetate / 1,4-dioxane / 100 °C / Inert atmosphere

2: sodium periodate; ammonium acetate / water; acetone / 20 °C

With sodium periodate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; ammonium acetate; potassium acetate; In 1,4-dioxane; water; acetone;
DOI:10.1021/jm800222k

Reference yield:

: 19520-74-2
3-hydroxy-5-methoxy-benzoic acid methyl ester

: 1048330-11-5
[3-methoxy-5-(methoxycarbonyl)phenyl]boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 4 - 20 °C / Inert atmosphere

2: 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; potassium acetate / 1,4-dioxane / 100 °C / Inert atmosphere

3: sodium periodate; ammonium acetate / water; acetone / 20 °C

With 2,6-dimethylpyridine; sodium periodate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(ii)dichloride-chloroform adduct; ammonium acetate; potassium acetate; In 1,4-dioxane; dichloromethane; water; acetone;
DOI:10.1021/jm800222k