Methylbis(di(2-methoxyphenyl)phosphino)amine

Base Information

Chemical Name:Methylbis(di(2-methoxyphenyl)phosphino)amine
CAS No.:197798-18-8
Molecular Formula:C29H31NO4P2
Molecular Weight:519.517
Hs Code.:
Mol file:197798-18-8.mol

Synonyms:Methylbis(di(2-methoxyphenyl)phosphino)amine

Suppliers and Price of Methylbis(di(2-methoxyphenyl)phosphino)amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 17 raw suppliers

Chemical Property of Methylbis(di(2-methoxyphenyl)phosphino)amine

Chemical Property:

PSA：67.34000
LogP:5.04840

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

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Technology Process of Methylbis(di(2-methoxyphenyl)phosphino)amine

There total 3 articles about Methylbis(di(2-methoxyphenyl)phosphino)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: P(2-methoxyphenyl)2Br

: 263369-88-6
di-o-anisylphosphinyl chloride

: 74-89-5
methylamine

: 197798-18-8
N-[bis(2-methoxyphenyl)phosphino]-P,P-bis(2-methoxyphenyl)-N-methylphosphinous amide

Guidance literature:: With triethylamine; In tetrahydrofuran; for 5h; Heating / reflux;

Reference yield: 56.0%

: 593-51-1
methylamine hydrochloride

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 197798-18-8
N-[bis(2-methoxyphenyl)phosphino]-P,P-bis(2-methoxyphenyl)-N-methylphosphinous amide

Guidance literature:: 2-methoxyphenylmagnesium bromide; With phosphorus tribromide; In tetrahydrofuran; at -78 - 20 ℃; for 19.5h; Glovebox; Inert atmosphere;

methylamine hydrochloride; With triethylamine; In tetrahydrofuran; for 24h; Glovebox; Inert atmosphere;
DOI:10.1021/acs.organomet.9b00721