3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER

Base Information

Chemical Name:3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER
CAS No.:82673-71-0
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:
Mol file:82673-71-0.mol

Synonyms:3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER

Suppliers and Price of 3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]ACRYLIC ACID ETHYL ESTER 95.00%
5MG
$ 497.31

Total 3 raw suppliers

Chemical Property of 3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER

Chemical Property:

PSA：64.63000
LogP:3.32910

Purity/Quality:: 3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]ACRYLIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER

There total 3 articles about 3-[2-(2,2-DIMETHYL-PROPIONYLAMINO)-6-METHOXY-PHENYL]-ACRYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 82673-65-2
N-(2-formyl-3-methoxyphenyl)pivalamide

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 82673-71-0,82673-76-5
ethyl (2-methoxy-6-pivaloylamino)cinnamate

Guidance literature:: In benzene; for 2h; Ambient temperature;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 82673-71-0,82673-76-5
ethyl (2-methoxy-6-pivaloylamino)cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N; 2.) n-BuLi / 1.) hexane, tetrahydrofuran, 0 deg C, 2 h; 2.) dimethylformamide, 0 deg C, 1 h; room temp., 8 h

2: 77 percent / benzene / 2 h / Ambient temperature

With n-butyllithium; triethylamine; In benzene;

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 82673-71-0,82673-76-5
ethyl (2-methoxy-6-pivaloylamino)cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N; 2.) n-BuLi / 1.) hexane, tetrahydrofuran, 0 deg C, 2 h; 2.) dimethylformamide, 0 deg C, 1 h; room temp., 8 h

2: 77 percent / benzene / 2 h / Ambient temperature

With n-butyllithium; triethylamine; In benzene;