Dichloroplatinum(2+);dimethylazanide

Base Information

• Chemical Name: Dichloroplatinum(2+);dimethylazanide
• CAS No.: 27928-80-9
• Molecular Formula: C₄H₁₄Cl₂N₂Pt
• Molecular Weight: 356.155
• DSSTox Substance ID: DTXSID90329757
• Mol file: 27928-80-9.mol

Synonyms:DTXSID90329757

Chemical Property of Dichloroplatinum(2+);dimethylazanide

Chemical Property:

• Vapor Pressure: 1520mmHg at 25°C
• Boiling Point: 6.1°Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 353.002548
• Heavy Atom Count: 9
• Complexity: 5.5

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N-]C.C[N-]C.Cl[Pt+2]Cl

Technology Process of Dichloroplatinum(2+);dimethylazanide

There total 4 articles about Dichloroplatinum(2+);dimethylazanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

potassium tetrachloroplatinate(II) (10025-99-7) + dimethyl amine (124-40-3) → cis-[PtCl2(dma)2] (26047-49-4,27928-80-9,92283-17-5)

Guidance literature:

In water; addn. of an aq. dimethylamine-soln. to a 10% K2(PtCl4)-soln.; pptn. in 6 h;;

DOI:10.1039/JR9320002975

Reference yield: 33.0%

potassium tetrachloroplatinate(II) (10025-99-7) + N,N-dimethylammonium chloride (506-59-2) → cis-[PtCl2(dma)2] (26047-49-4,27928-80-9,92283-17-5) + trans-Pt((CH3)2NH)2Cl2 (26047-49-4,92283-17-5,27928-80-9)

Guidance literature:

With NaOH; HCl; In water; stirred at room temp. for 6 h; cooling on ice bath;; cis-complex filtered,washed (Me2CO),dissolved (H2O),filtered;cooled;concd. HCl added;crystn.;trans-complex: NaOH added to filtrate and evapd. washings;evapn. (water-bath);addn.of concd.HCl;heated (2 h);crystn.;crystals washed (H2O) and dried;elem. anal.;

DOI:10.1016/S0020-1693(00)83355-1

Reference yield: 33.0%

potassium tetrachloroplatinate(II) (10025-99-7) + N,N-dimethylammonium chloride (506-59-2) → cis-[PtCl2(dma)2] (26047-49-4,27928-80-9,92283-17-5) + trans-Pt((CH3)2NH)2Cl2 (26047-49-4,92283-17-5,27928-80-9)

Guidance literature:

With NaOH; HCl; In water; stirred at room temp. for 6 h; cooling on ice bath;; cis-complex filtered,washed (Me2CO),dissolved (H2O),filtered;cooled;concd. HCl added;crystn.;trans-complex: NaOH added to filtrate and evapd. washings;evapn. (water-bath);addn.of concd.HCl;heated (2 h);crystn.;crystals washed (H2O) and dried;elem. anal.;

DOI:10.1016/S0020-1693(00)83355-1

upstream raw materials:

potassium tetrachloroplatinate(II)

N,N-dimethylammonium chloride

dimethyl amine

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