Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI)

Base Information

• Chemical Name: Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI)
• CAS No.: 40477-79-0
• Molecular Formula: C₆H₄Cl₂O
• Molecular Weight: 163.003
• Mol file: 40477-79-0.mol

Synonyms:Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI)

Chemical Property of Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI)

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

2,4-DICHLOROPHENOL-[14C(U)] 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xn
• Statements: 11-38-48/20-63-65-67
• Safety Statements: 36/37-62

MSDS Files:

Useful:

Technology Process of Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI)

There total 151 articles about Phenol, 2,4-dichloro-, labeled with carbon-14 (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-chloro-phenol (106-48-9,82344-39-6) → 2,4-dichlorophenol (120-83-2,40477-79-0) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8)

Guidance literature:

With hydrogenchloride; 3-chloro-benzenecarboperoxoic acid; In N,N-dimethyl-formamide; for 0.333333h; Product distribution; Ambient temperature; other phenols;

Reference yield: 18.4%

phenol (108-95-2,27073-41-2) → 2,6-Dichlorophenol (87-65-0) + 2-monochlorophenol (95-57-8) + 4-chloro-phenol (106-48-9,82344-39-6) + 2,4-dichlorophenol (120-83-2,40477-79-0) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8)

Guidance literature:

With aluminium trichloride; diphenyl sulfide; chlorine; In neat (no solvent); at 35 ℃; for 1.5h; Product distribution; others 2-alkylphenols; var. chlorinating agent, temp., and time;

DOI:10.1021/jo00212a029

Reference yield: 6.0%

phenol (108-95-2,27073-41-2) → 2,4-dichlorophenol (120-83-2,40477-79-0) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8)

Guidance literature:

With hydrogenchloride; sodium chlorate; In water; acetic acid; at 20 ℃; for 26h;

DOI:10.5012/bkcs.2011.32.2.472

upstream raw materials:

1-bromo-2,4-dichlorobenzene

sodium methylate

ethanol

2,4-dichlorophenoxymethyl chloride

Downstream raw materials:

furan-2-carboxylic acid-(2,4-dichloro-phenyl ester)

2-chloro-4-chlorophenyl 4-chlorobenzoate

1-chloro-3-(2,4-dichloro-phenoxy)-propan-2-ol

Methoxymethyl-carbamic acid 2,4-dichloro-phenyl ester

Refernces

• 1、 Jana, Rahul Dev,Munshi, Sandip,Paine, Tapan Kanti. "Oxidative degradation of toxic organic pollutants by water soluble nonheme iron(iv)-oxo complexes of polydentate nitrogen donor ligands". . p. 5590 - 5597. Retrieved 2021/05/04.
• 2、 Lam, Sze-Mun,Jaffari, Zeeshan Haider,Sin, Jin-Chung,Zeng, Honghu,Lin, Hua,Li, Haixiang,Mohamed, Abdul Rahman,Ng, Ding-Quan. "Surface decorated coral-like magnetic BiFeO3 with Au nanoparticles for effective sunlight photodegradation of 2,4-D and E. coli inactivation". . . Retrieved 2021/01/26.