Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-

Base Information

Chemical Name:Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-
CAS No.:125158-55-6
Molecular Formula:C18H23NO5
Molecular Weight:333.384
Hs Code.:
Mol file:125158-55-6.mol

Synonyms:Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-

Suppliers and Price of Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-

Chemical Property:

PSA：58.51000
LogP:1.70100

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.-

There total 2 articles about Furo3,2-doxazole, 5-(2,2-dimethyl-1,3-dioxolan-4-yl)-3a,5,6,6a-tetrahydro-2-methyl-6-(phenylmethoxy)-, 3aR-3a.alpha.,5.alpha.(R*),6.alpha.,6a.alpha.- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 100-39-0
benzyl bromide

: 117177-19-2
2-methyl-(1,2-dideoxy-5,6-O-isopropylidene-α-D-glucofurano)-<2,1-d>-2-oxazoline

: 125158-55-6
2-methyl-(3-O-benzyl-1,2-dideoxy-5,6-O-isopropylidene-α-D-glucofurano)-<2.1-d>-2-oxazoline

Guidance literature:: 2-methyl-(1,2-dideoxy-5,6-O-isopropylidene-α-D-glucofurano)-<2,1-d>-2-oxazoline; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo801927k

Reference yield:

: 7512-17-6,282727-46-2,478518-83-1,127959-06-2,78393-48-3
2-acetamido-2-deoxy-D-glucose

: 100-39-0
benzyl bromide

: 67-64-1
acetone

: 125158-55-6
2-methyl-(3-O-benzyl-1,2-dideoxy-5,6-O-isopropylidene-α-D-glucofurano)-<2.1-d>-2-oxazoline

Guidance literature:: 2-acetamido-2-deoxy-D-glucose; acetone; With iron(III) chloride; for 0.5h; Reflux;

benzyl bromide; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 4h;
DOI:10.3987/COM-12-S(N)69