tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Base Information

Chemical Name:tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate
CAS No.:1356009-27-2
Molecular Formula:C₁₇H₂₃N₅O₅
Molecular Weight:377.4
Hs Code.:
Mol file:1356009-27-2.mol

Synonyms:tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Suppliers and Price of tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

There total 7 articles about tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.8%

: 1356009-25-0
2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenol

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1356009-27-2
tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 1356009-27-2
tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 18 h / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With carbon tetrabromide; caesium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1356009-27-2
tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 18 h / 0 - 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With carbon tetrabromide; caesium carbonate; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;