tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

Base Information

Chemical Name:tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate
CAS No.:1356009-29-4
Molecular Formula:C₁₈H₂₅N₅O₅
Molecular Weight:391.427
Hs Code.:

Synonyms:tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

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Chemical Property of tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

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Technology Process of tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

There total 9 articles about tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1356009-27-2
tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate

: 74-88-4
methyl iodide

: 1356009-29-4
tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

Guidance literature:: tert-butyl 3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propylcarbamate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 1356009-29-4
tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 18 h / 0 - 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

3.2: 1 h / 20 °C

With carbon tetrabromide; sodium hydride; caesium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1356009-29-4
tert-butyl methyl(3-(2-(3-methyl-1H-1,2,4-triazol-1-yl)-5-nitrophenoxy)propyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 18 h / 0 - 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

4.2: 1 h / 20 °C

With carbon tetrabromide; sodium hydride; caesium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;