N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine

Base Information

Chemical Name:N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine
CAS No.:1161432-26-3
Molecular Formula:C18H17N3
Molecular Weight:275.34768
Hs Code.:2933599090
Mol file:1161432-26-3.mol

Synonyms:N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine

Suppliers and Price of N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-Benzyl-1-phenyl-1-(pyrimidin-2-yl)methanamine 95+%
1g
$ 581.00

Chemenu
N-benzyl-1-phenyl-1-(pyrimidin-2-yl)methanamine 95%
1g
$ 549.00

Total 2 raw suppliers

Chemical Property of N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine

Chemical Property:

Melting Point:73 °C
Boiling Point:417.9±40.0 °C(Predicted)
PSA：37.81000
Density:1.137±0.06 g/cm3(Predicted)
LogP:3.74670

Purity/Quality:

≥99% ^*data from raw suppliers

N-Benzyl-1-phenyl-1-(pyrimidin-2-yl)methanamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine

There total 2 articles about N-Benzyl-1-phenyl-1-(pyriMidin-2-yl)MethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 907594-98-3
2-pyrimidylphenylmethylamine

: 100-52-7
benzaldehyde

: 1161432-26-3
N-benzyl-N-[phenyl(pyrimidin-2-yl)methyl]amine

Guidance literature:: 2-pyrimidylphenylmethylamine; benzaldehyde; With magnesium sulfate; In methanol; at 20 ℃; for 12h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;
DOI:10.1002/ejic.200800154

Reference yield:

: 14080-23-0
2-cyanopyrimidine

: 100-59-4
phenylmagnesium chloride

: 1161432-26-3
N-benzyl-N-[phenyl(pyrimidin-2-yl)methyl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: magnesium sulfate / methanol

With magnesium sulfate; In tetrahydrofuran; methanol;
DOI:10.1021/om200375s

Reference yield: 95.0%

: sodium tetrachloropalladate(II)

: 1161432-26-3
N-benzyl-N-[phenyl(pyrimidin-2-yl)methyl]amine

: 1161439-11-7
Cl₂Pd((C₄H₃N₂)(C₆H₅)CHNHCH₂(C₆H₅))

Guidance literature:: In methanol; Na2PdCl4 (0.25 mmol) added to soln. of amine (0.25 mmol); stirred (room temp., 16 h); solvent removed (vac.); residue filtered through silica gel pad by elution with cyclohexane/EtOAc (7:3) and then with EtOAc; elem. anal.;
DOI:10.1002/ejic.200800154