Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-

Base Information

Chemical Name:Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-
CAS No.:1338925-48-6
Molecular Formula:C13H16INO5
Molecular Weight:393.17431
Hs Code.:
Mol file:1338925-48-6.mol

Synonyms:Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-

Suppliers and Price of Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-

Chemical Property:

PSA：95.86000
LogP:3.03810

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo-

There total 2 articles about Be-nzenacetic acid,a-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-3-iodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69651-48-5
N-tert-butyloxycarbonyl-L-4-hydroxyphenylglycine

: 1338925-48-6
Boc-N-Me-3-Iodo-hydroxyphenylglycine

Guidance literature:: With sodium hypochlorite; sodium iodide; sodium hydroxide; In methanol; water; at 0 ℃; for 3h;
DOI:10.1021/ja207318n

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 32462-30-9
(S)-hydroxyphenylglycine

: 1338925-48-6
Boc-N-Me-3-Iodo-hydroxyphenylglycine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone

2: sodium hypochlorite; sodium iodide; sodium hydroxide / methanol; water / 3 h / 0 °C

With sodium hypochlorite; sodium hydrogencarbonate; sodium iodide; sodium hydroxide; In methanol; water; acetone;
DOI:10.1021/ja207318n

Reference yield:

: 1338925-48-6
Boc-N-Me-3-Iodo-hydroxyphenylglycine

: L-2-aminobutyric acid HCl

: 74-88-4
methyl iodide

: C₂₀H₂₉IN₂O₆

Guidance literature:: Boc-N-Me-3-Iodo-hydroxyphenylglycine; L-2-aminobutyric acid HCl; With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

methyl iodide; With potassium carbonate; In N,N-dimethyl-formamide; acetone; for 1.5h; Reflux; Sealed tube;