2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline

Base Information Edit

Chemical Name:2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline
CAS No.:14097-35-9
Molecular Formula:C₁₀H₁₂N₂O₂
Molecular Weight:192.217
Hs Code.:
Mol file:14097-35-9.mol

Synonyms:1,2,3,4-tetrahydro-2-methyl-7-nitroisoquinoline

Suppliers and Price of 2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline Edit

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Boiling Point:296.931°C at 760 mmHg
Flash Point:133.379°C
Density:1.208g/cm³

Purity/Quality:: 98.5% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline

There total 11 articles about 2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 64-18-6
formic acid

: 42923-79-5
7-nitro-1,2,3,4-tetrahydroisoquinoline

: 14097-35-9
2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: formic acid; With acetic anhydride; at 0 - 50 ℃; for 0.75h;

7-nitro-1,2,3,4-tetrahydroisoquinoline; In tetrahydrofuran; at -18 - -15 ℃; for 0.5h;

With dimethylsulfide borane complex; In tetrahydrofuran; at 10 - 20 ℃; for 1h;
DOI:10.1021/jm800967h

Reference yield: 85.0%

: 42923-79-5
7-nitro-1,2,3,4-tetrahydroisoquinoline

: 14097-35-9
2-methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: formic acid; With acetic anhydride; at 0 - 50 ℃; for 0.75h;

7-nitro-1,2,3,4-tetrahydroisoquinoline; In tetrahydrofuran; at -18 - -15 ℃; for 0.5h;

With hydrogenchloride; BH_3.DMS; more than 3 stages;