6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester

Base Information

Chemical Name:6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester
CAS No.:1313498-27-9
Molecular Formula:C9H15NO3
Molecular Weight:185.2203
Hs Code.:
Mol file:1313498-27-9.mol

Synonyms:6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester;ethyl 6-methoxy-2,3,4,5-tetrahydropyridine-4-carboxylate

Suppliers and Price of 6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester

Chemical Property:

PSA：47.89000
LogP:0.44000

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester

There total 3 articles about 6-Methoxy-2,3,4,5-tetrahydro-pyridine-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 420-37-1
trimethoxonium tetrafluoroborate

: 25410-09-7
ethyl 2-oxopiperidine-4-carboxylate

: 1313498-27-9
2-methoxy-3,4,5,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: In dichloromethane; at 0 ℃; for 3h; Product distribution / selectivity;

Reference yield:

: 1313498-26-8
1-tert-butyl 4-ethyl 2-oxopiperidine-1,4-dicarboxylate

: 1313498-27-9
2-methoxy-3,4,5,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h

2: dichloromethane / 3 h / 0 °C

With hydrogenchloride; In 1,4-dioxane; dichloromethane;

Reference yield:

: 142851-03-4
1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate

: 1313498-27-9
2-methoxy-3,4,5,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium periodate; ruthenium(IV) oxide hydrate / acetonitrile; water / 1.5 h / 20 - 35 °C

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h

3: dichloromethane / 3 h / 0 °C

With hydrogenchloride; sodium periodate; ruthenium(IV) oxide hydrate; In 1,4-dioxane; dichloromethane; water; acetonitrile;