6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one

Base Information

Chemical Name:6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one
CAS No.:134894-53-4
Molecular Formula:C14H12N2O2
Molecular Weight:240.2573
Hs Code.:
Mol file:134894-53-4.mol

Synonyms:6,9DiMe-PBOA-5one;6,9-Dimethyl-pyrido[2,3-b][1,5]benzoxazepin-5(6H)-one;

Suppliers and Price of 6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one

Chemical Property:

Vapor Pressure:9.55E-08mmHg at 25°C
Boiling Point:434.3°Cat760mmHg
Flash Point:216.5°C
PSA：42.43000
Density:1.251g/cm³
LogP:2.83730

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one

There total 4 articles about 6,9-dimethylpyrido[2,3-b][1,5]benzoxazepin-5(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 134894-53-4
7,10-Dimethyl-10H-5-oxa-4,10-diaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: Multi-step reaction with 3 steps

1: 27 percent / (i-Pr)2NEt / ethyl acetate / 2 h / 0 °C

2: 80 percent / NaOH / dimethylformamide / 5 h / 120 °C

3: NaH / dimethylformamide / Ambient temperature

With sodium hydroxide; sodium hydride; N-ethyl-N,N-diisopropylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00088a027

Reference yield:

: 2835-98-5
2-Hydroxy-4-methylanilin

: 134894-53-4
7,10-Dimethyl-10H-5-oxa-4,10-diaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: Multi-step reaction with 3 steps

1: 27 percent / (i-Pr)2NEt / ethyl acetate / 2 h / 0 °C

2: 80 percent / NaOH / dimethylformamide / 5 h / 120 °C

3: NaH / dimethylformamide / Ambient temperature

With sodium hydroxide; sodium hydride; N-ethyl-N,N-diisopropylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00088a027

Reference yield:

: 140413-43-0
2-Chloro-N-(2-hydroxy-4-methyl-phenyl)-nicotinamide

: 134894-53-4
7,10-Dimethyl-10H-5-oxa-4,10-diaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOH / dimethylformamide / 5 h / 120 °C

2: NaH / dimethylformamide / Ambient temperature

With sodium hydroxide; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm00088a027